6-[(3-chlorophenyl)methyl]-4H-[1,2,4]triazolo[1,5-a]pyrimidine-5,7-dione tri-n-butylamine salt

Base Information

Chemical Name:6-[(3-chlorophenyl)methyl]-4H-[1,2,4]triazolo[1,5-a]pyrimidine-5,7-dione tri-n-butylamine salt
CAS No.:1335027-61-6
Molecular Formula:C₁₂H₉ClN₄O₂*C₁₂H₂₇N
Molecular Weight:462.035
Hs Code.:

Synonyms:6-[(3-chlorophenyl)methyl]-4H-[1,2,4]triazolo[1,5-a]pyrimidine-5,7-dione tri-n-butylamine salt

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Chemical Property of 6-[(3-chlorophenyl)methyl]-4H-[1,2,4]triazolo[1,5-a]pyrimidine-5,7-dione tri-n-butylamine salt

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Technology Process of 6-[(3-chlorophenyl)methyl]-4H-[1,2,4]triazolo[1,5-a]pyrimidine-5,7-dione tri-n-butylamine salt

There total 2 articles about 6-[(3-chlorophenyl)methyl]-4H-[1,2,4]triazolo[1,5-a]pyrimidine-5,7-dione tri-n-butylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 102-82-9
tributyl-amine

: 70146-77-9
[(3-chlorophenyl)methyl]propanedioic acid dirthyl ester

: 61-82-5
3-amino-1,2,4-triazole

: 1335027-61-6
6-[(3-chlorophenyl)methyl]-4H-[1,2,4]triazolo[1,5-a]pyrimidine-5,7-dione tri-n-butylamine salt

Guidance literature:: at 180 ℃; for 6h;

Reference yield:

: 766-80-3
1-bromomethyl-3-chlorobenzene

: 1335027-61-6
6-[(3-chlorophenyl)methyl]-4H-[1,2,4]triazolo[1,5-a]pyrimidine-5,7-dione tri-n-butylamine salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C

2.1: 6 h / 180 °C

With sodium hydride; In tetrahydrofuran; mineral oil;