(S)-2-(allylamino)-N-(2-((1S,2S)-3-(allyloxy)-1,2-dimethoxypropyl)phenyl)-3-methylbutanamide

Base Information

Chemical Name:(S)-2-(allylamino)-N-(2-((1S,2S)-3-(allyloxy)-1,2-dimethoxypropyl)phenyl)-3-methylbutanamide
CAS No.:1421051-46-8
Molecular Formula:C₂₂H₃₄N₂O₄
Molecular Weight:390.523
Hs Code.:

Synonyms:(S)-2-(allylamino)-N-(2-((1S,2S)-3-(allyloxy)-1,2-dimethoxypropyl)phenyl)-3-methylbutanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(allylamino)-N-(2-((1S,2S)-3-(allyloxy)-1,2-dimethoxypropyl)phenyl)-3-methylbutanamide

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Technology Process of (S)-2-(allylamino)-N-(2-((1S,2S)-3-(allyloxy)-1,2-dimethoxypropyl)phenyl)-3-methylbutanamide

There total 4 articles about (S)-2-(allylamino)-N-(2-((1S,2S)-3-(allyloxy)-1,2-dimethoxypropyl)phenyl)-3-methylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₉NO₅

: 1421051-46-8
(S)-2-(allylamino)-N-(2-((1S,2S)-3-(allyloxy)-1,2-dimethoxypropyl)phenyl)-3-methylbutanamide

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; zinc / ethanol / 0.5 h / 0 - 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 3 h / 20 °C

3: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.08 h / 20 °C

4: triethylamine / methanol / 12 h / Reflux

With acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; zinc; In tetrahydrofuran; methanol; ethanol; acetonitrile;
DOI:10.1021/ol3032126

Reference yield:

: 1421051-27-5
2-((1S,2S)-3-(allyloxy)-1,2-dimethoxypropyl)aniline

: 1421051-46-8
(S)-2-(allylamino)-N-(2-((1S,2S)-3-(allyloxy)-1,2-dimethoxypropyl)phenyl)-3-methylbutanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 3 h / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.08 h / 20 °C

3: triethylamine / methanol / 12 h / Reflux

With 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ol3032126

Reference yield:

: 1421051-33-3
(9H-fluoren-9-yl)methyl (S)-1-(2-((1S,2S)-3-(allyloxy)-1,2-dimethoxypropyl)phenylamino)-3-methyl-1-oxobutan-2-ylcarbamate

: 1421051-46-8
(S)-2-(allylamino)-N-(2-((1S,2S)-3-(allyloxy)-1,2-dimethoxypropyl)phenyl)-3-methylbutanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.08 h / 20 °C

2: triethylamine / methanol / 12 h / Reflux

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1021/ol3032126