sodium (1S,2R)-1-(3-bromophenyl)-2-(hydroxymethyl)cyclopropanecarboxylate

Base Information

Chemical Name:sodium (1S,2R)-1-(3-bromophenyl)-2-(hydroxymethyl)cyclopropanecarboxylate
CAS No.:1402883-80-0
Molecular Formula:C₁₁H₁₀BrO₃*Na
Molecular Weight:293.092
Hs Code.:

Synonyms:sodium (1S,2R)-1-(3-bromophenyl)-2-(hydroxymethyl)cyclopropanecarboxylate

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Chemical Property of sodium (1S,2R)-1-(3-bromophenyl)-2-(hydroxymethyl)cyclopropanecarboxylate

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Technology Process of sodium (1S,2R)-1-(3-bromophenyl)-2-(hydroxymethyl)cyclopropanecarboxylate

There total 2 articles about sodium (1S,2R)-1-(3-bromophenyl)-2-(hydroxymethyl)cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1402883-78-6
(1S,5R)-1-(3-bromophenyl)-3-oxabicyclo[3.1.0]hexan-2-one

: 1402883-80-0
sodium (1S,2R)-1-(3-bromophenyl)-2-(hydroxymethyl)cyclopropanecarboxylate

Guidance literature:: (1S,5R)-1-(3-bromophenyl)-3-oxabicyclo[3.1.0]hexan-2-one; With potassium hydroxide; In ethanol; water; at 20 ℃;

With sodium methylate; In diethyl ether;
DOI:10.1021/jm3011405

Reference yield:

: 31938-07-5
(3-bromophenyl)acetonitrile

: 1402883-80-0
sodium (1S,2R)-1-(3-bromophenyl)-2-(hydroxymethyl)cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium amide / benzene / 1 h / 20 °C / Cooling with ice

1.2: 0.83 h / 20 °C / Cooling with ice

1.3: 8 h / Reflux

2.1: potassium hydroxide / ethanol; water / 20 °C

With sodium amide; potassium hydroxide; In ethanol; water; benzene;
DOI:10.1021/jm3011405