3-[1-(3-Fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-(trifluoromethyl)propanal

Base Information

• Chemical Name: 3-[1-(3-Fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-(trifluoromethyl)propanal
• CAS No.: 850564-85-1
• Molecular Formula: C₁₄H₁₄F₄O₃
• Molecular Weight: 306.257

Synonyms:3-[1-(3-Fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-(trifluoromethyl)propanal

Chemical Property of 3-[1-(3-Fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-(trifluoromethyl)propanal

Chemical Property:

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Technology Process of 3-[1-(3-Fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-(trifluoromethyl)propanal

There total 1 articles about 3-[1-(3-Fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-(trifluoromethyl)propanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-[1-(3-fluoro-2-methoxyphenyl)-cyclopropyl]-2-trifluoromethyl-propane-1,2-diol (850564-87-3) → 3-[1-(3-Fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-(trifluoromethyl)propanal (850564-85-1)

Guidance literature:

With sulfur trioxide pyridine complex; triethylamine; In dichloromethane; dimethyl sulfoxide; for 3h;

Reference yield:

5-amino-8-fluoro-2-methyl-quinazoline (825654-53-3) + 3-[1-(3-Fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-(trifluoromethyl)propanal (850564-85-1) → 1-[(8-fluoro-2-methylquinazolin-5-yl)imino]-3-[1-(3-fluoro-2-methoxyphenyl)-cyclopropyl]-2-trifluoromethylpropan-2-ol

Guidance literature:

With titanium(IV) tetraethanolate; In toluene; at 100 ℃; for 2h;

Reference yield:

5-aminoquinolin-2(1H)-one (61317-32-6) + 3-[1-(3-Fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-(trifluoromethyl)propanal (850564-85-1) → 5-[3-[1-(3-fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-trifluoromethyl-propylimino]-quinolin-2(1H)-one (879339-22-7)

Guidance literature:

With titanium(IV) tetraethanolate; In toluene; at 100 ℃; for 1h;

upstream raw materials:

3-[1-(3-fluoro-2-methoxyphenyl)-cyclopropyl]-2-trifluoromethyl-propane-1,2-diol

Downstream raw materials:

3-[1-(3-fluoro-2-methoxyphenyl)-cyclopropyl]-1-[(2-methylquinazolin-5-yl)imino]-2-trifluoromethylpropan-2-ol

5-[3-[1-(3-fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-trifluoromethyl-propylimino]-2-methylphthalazin-1-one

5-[3-[1-(3-fluoro-2-methoxyphenyl)-cyclopropyl]-2-hydroxy-2-trifluoromethyl-propylimino]-quinolin-2(1H)-one

3-[1-(3-fluoro-2-methoxyphenyl)-cyclopropyl]-1-[(2-methylquinolin-5-yl)imino]-2-trifluoromethyl-propan-2-ol

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