N-[3-benzenesulfinylmethyl-5-(2-fluorophenyl)-3H-1,2,3-triazol-4-yl]-2-chloro-2-cyclobutylacetamide

Base Information

Chemical Name:N-[3-benzenesulfinylmethyl-5-(2-fluorophenyl)-3H-1,2,3-triazol-4-yl]-2-chloro-2-cyclobutylacetamide
CAS No.:252369-30-5
Molecular Formula:C₂₁H₂₀ClFN₄O₂S
Molecular Weight:446.933
Hs Code.:

Synonyms:N-[3-benzenesulfinylmethyl-5-(2-fluorophenyl)-3H-1,2,3-triazol-4-yl]-2-chloro-2-cyclobutylacetamide

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Chemical Property of N-[3-benzenesulfinylmethyl-5-(2-fluorophenyl)-3H-1,2,3-triazol-4-yl]-2-chloro-2-cyclobutylacetamide

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Technology Process of N-[3-benzenesulfinylmethyl-5-(2-fluorophenyl)-3H-1,2,3-triazol-4-yl]-2-chloro-2-cyclobutylacetamide

There total 5 articles about N-[3-benzenesulfinylmethyl-5-(2-fluorophenyl)-3H-1,2,3-triazol-4-yl]-2-chloro-2-cyclobutylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 252369-29-2
2-chloro-2-cyclobutyl-N-[5-(2-fluorophenyl)-3-phenylsulfenylmethyl-3H-1,2,3-triazol-4-yl]acetamide

: 252369-30-5
N-[3-benzenesulfinylmethyl-5-(2-fluorophenyl)-3H-1,2,3-triazol-4-yl]-2-chloro-2-cyclobutylacetamide

Guidance literature:: With ozone; In dichloromethane; at -78 ℃;
DOI:10.1055/s-2001-13354

Reference yield:

: 77422-70-9
azidomethyl phenyl sulphide

: 252369-30-5
N-[3-benzenesulfinylmethyl-5-(2-fluorophenyl)-3H-1,2,3-triazol-4-yl]-2-chloro-2-cyclobutylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 29 percent / K₂CO₃ / dimethylsulfoxide / 16 h / 20 °C

2: 31 percent / pyridine / dimethylformamide / 0 °C

3: O₃ / CH₂Cl₂ / -78 °C

With pyridine; potassium carbonate; ozone; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1055/s-2001-13354

Reference yield:

: 326-62-5
2-fluorophenyl acetonitrile

: 252369-30-5
N-[3-benzenesulfinylmethyl-5-(2-fluorophenyl)-3H-1,2,3-triazol-4-yl]-2-chloro-2-cyclobutylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 29 percent / K₂CO₃ / dimethylsulfoxide / 16 h / 20 °C

2: 31 percent / pyridine / dimethylformamide / 0 °C

3: O₃ / CH₂Cl₂ / -78 °C

With pyridine; potassium carbonate; ozone; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1055/s-2001-13354