N-{3-[2-(2-chloro-acetylamino)-4,5,6,7-tetrahydro-benzo [b]thiophen-3-ylmethyl]-5-hydrazinocarbonylmethylsulfanyl-[1,2,4]triazol-4-yl}-benzamide

Base Information

Chemical Name:N-{3-[2-(2-chloro-acetylamino)-4,5,6,7-tetrahydro-benzo [b]thiophen-3-ylmethyl]-5-hydrazinocarbonylmethylsulfanyl-[1,2,4]triazol-4-yl}-benzamide
CAS No.:1310547-11-5
Molecular Formula:C₂₂H₂₄ClN₇O₃S₂
Molecular Weight:534.063
Hs Code.:

Synonyms:N-{3-[2-(2-chloro-acetylamino)-4,5,6,7-tetrahydro-benzo [b]thiophen-3-ylmethyl]-5-hydrazinocarbonylmethylsulfanyl-[1,2,4]triazol-4-yl}-benzamide

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Chemical Property of N-{3-[2-(2-chloro-acetylamino)-4,5,6,7-tetrahydro-benzo [b]thiophen-3-ylmethyl]-5-hydrazinocarbonylmethylsulfanyl-[1,2,4]triazol-4-yl}-benzamide

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Technology Process of N-{3-[2-(2-chloro-acetylamino)-4,5,6,7-tetrahydro-benzo [b]thiophen-3-ylmethyl]-5-hydrazinocarbonylmethylsulfanyl-[1,2,4]triazol-4-yl}-benzamide

There total 6 articles about N-{3-[2-(2-chloro-acetylamino)-4,5,6,7-tetrahydro-benzo [b]thiophen-3-ylmethyl]-5-hydrazinocarbonylmethylsulfanyl-[1,2,4]triazol-4-yl}-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1310546-99-6
{4-benzoylamino-5-[2-(2-chloro-acetylamino)-4,5,6,7-tetrahydro-benzo[b]thiophen-3-ylmethyl]-4H-[1,2,4]triazol-3-ylsulfanyl}-acetic acid methyl ester

: 1310547-11-5
N-{3-[2-(2-chloro-acetylamino)-4,5,6,7-tetrahydro-benzo [b]thiophen-3-ylmethyl]-5-hydrazinocarbonylmethylsulfanyl-[1,2,4]triazol-4-yl}-benzamide

Guidance literature:: With aluminum oxide; hydrazine hydrate; Microwave irradiation;
DOI:10.1016/j.ejmech.2011.02.059

Reference yield:

: C₁₂H₁₆ClN₃O₂S

: 1310547-11-5
N-{3-[2-(2-chloro-acetylamino)-4,5,6,7-tetrahydro-benzo [b]thiophen-3-ylmethyl]-5-hydrazinocarbonylmethylsulfanyl-[1,2,4]triazol-4-yl}-benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hydroxide

2: hydrazine hydrate

3: sodium hydroxide / 0 °C

4: aluminum oxide; sodium hydroxide / Microwave irradiation

5: aluminum oxide; hydrazine hydrate / Microwave irradiation

With aluminum oxide; hydrazine hydrate; potassium hydroxide; sodium hydroxide;
DOI:10.1016/j.ejmech.2011.02.059

Reference yield:

: 1310546-63-4
N-{3-[2-(2-chloro-acetylamino)-4,5,6,7-tetrahydro-benzo[b]thiophen-3-ylmethyl]-5-mercapto-[1,2,4]triazol-4-yl}-benzamide

: 1310547-11-5
N-{3-[2-(2-chloro-acetylamino)-4,5,6,7-tetrahydro-benzo [b]thiophen-3-ylmethyl]-5-hydrazinocarbonylmethylsulfanyl-[1,2,4]triazol-4-yl}-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum oxide; sodium hydroxide / Microwave irradiation

2: aluminum oxide; hydrazine hydrate / Microwave irradiation

With aluminum oxide; hydrazine hydrate; sodium hydroxide;
DOI:10.1016/j.ejmech.2011.02.059