4-bromo-3-[5-(diethoxymethyl)fur-2-yl]-2,5-dihydro-1-benzyl-1H-pyrrole-2,5-dione

Base Information

Chemical Name:4-bromo-3-[5-(diethoxymethyl)fur-2-yl]-2,5-dihydro-1-benzyl-1H-pyrrole-2,5-dione
CAS No.:853649-61-3
Molecular Formula:C₂₀H₂₀BrNO₅
Molecular Weight:434.286
Hs Code.:

Synonyms:4-bromo-3-[5-(diethoxymethyl)fur-2-yl]-2,5-dihydro-1-benzyl-1H-pyrrole-2,5-dione

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Chemical Property of 4-bromo-3-[5-(diethoxymethyl)fur-2-yl]-2,5-dihydro-1-benzyl-1H-pyrrole-2,5-dione

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Technology Process of 4-bromo-3-[5-(diethoxymethyl)fur-2-yl]-2,5-dihydro-1-benzyl-1H-pyrrole-2,5-dione

There total 5 articles about 4-bromo-3-[5-(diethoxymethyl)fur-2-yl]-2,5-dihydro-1-benzyl-1H-pyrrole-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 853649-60-2
3-[5-(diethoxymethyl)fur-2-yl]-2,5-dihydro-1-benzyl-1H-pyrrole-2,5-dione

: 853649-61-3
4-bromo-3-[5-(diethoxymethyl)fur-2-yl]-2,5-dihydro-1-benzyl-1H-pyrrole-2,5-dione

Guidance literature:: 3-[5-(diethoxymethyl)fur-2-yl]-2,5-dihydro-1-benzyl-1H-pyrrole-2,5-dione; With bromine; In dichloromethane; at 0 ℃;

With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tet.2005.03.016

Reference yield:

: 13529-27-6
2-(diethoxymethyl)furan

: 853649-61-3
4-bromo-3-[5-(diethoxymethyl)fur-2-yl]-2,5-dihydro-1-benzyl-1H-pyrrole-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: bromine / CH₂Cl₂ / 0 °C

1.2: 70 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With bromine; In dichloromethane;
DOI:10.1016/j.tet.2005.03.016

Reference yield:

: 122-51-0
orthoformic acid triethyl ester

: 853649-61-3
4-bromo-3-[5-(diethoxymethyl)fur-2-yl]-2,5-dihydro-1-benzyl-1H-pyrrole-2,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: 99 percent / ammonium chloride / ethanol / 16 h / Heating

2.1: bromine / CH₂Cl₂ / 0 °C

2.2: 70 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With ammonium chloride; bromine; In ethanol; dichloromethane;
DOI:10.1016/j.tet.2005.03.016