4-benzyl-1-[(2E)-3-(3-bromo-4-hydroxy-5-methoxyphenyl)prop-2-enoyl]piperazine hydrochloride

Base Information

Chemical Name:4-benzyl-1-[(2E)-3-(3-bromo-4-hydroxy-5-methoxyphenyl)prop-2-enoyl]piperazine hydrochloride
CAS No.:1467118-58-6
Molecular Formula:C₂₁H₂₃BrN₂O₃*ClH
Molecular Weight:467.79
Hs Code.:

Synonyms:4-benzyl-1-[(2E)-3-(3-bromo-4-hydroxy-5-methoxyphenyl)prop-2-enoyl]piperazine hydrochloride

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Chemical Property of 4-benzyl-1-[(2E)-3-(3-bromo-4-hydroxy-5-methoxyphenyl)prop-2-enoyl]piperazine hydrochloride

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Technology Process of 4-benzyl-1-[(2E)-3-(3-bromo-4-hydroxy-5-methoxyphenyl)prop-2-enoyl]piperazine hydrochloride

There total 2 articles about 4-benzyl-1-[(2E)-3-(3-bromo-4-hydroxy-5-methoxyphenyl)prop-2-enoyl]piperazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₅BrN₂O₄

: 1467118-58-6
4-benzyl-1-[(2E)-3-(3-bromo-4-hydroxy-5-methoxyphenyl)prop-2-enoyl]piperazine hydrochloride

Guidance literature:: C₂₃H₂₅BrN₂O₄; With sodium hydroxide; In ethanol; for 0.25h; Reflux;

With hydrogenchloride; In ethanol; at 5 ℃; for 72h;
DOI:10.3184/174751913X13700888313361

Reference yield:

: 691005-51-3
3-(3-bromo-4-acetyloxy-5-methoxyphenyl)-2-propenoic acid

: 1467118-58-6
4-benzyl-1-[(2E)-3-(3-bromo-4-hydroxy-5-methoxyphenyl)prop-2-enoyl]piperazine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride; pyridine / chloroform / 20 °C

2.1: triethylamine / chloroform / 20 °C

3.1: sodium hydroxide / ethanol / 0.25 h / Reflux

3.2: 72 h / 5 °C

With pyridine; oxalyl dichloride; triethylamine; sodium hydroxide; In ethanol; chloroform;
DOI:10.3184/174751913X13700888313361