methyl (phenyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate

Base Information

Chemical Name:methyl (phenyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate
CAS No.:725228-92-2
Molecular Formula:C₂₉H₃₀O₇S
Molecular Weight:522.619
Hs Code.:

Synonyms:methyl (phenyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (phenyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate

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Technology Process of methyl (phenyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate

There total 3 articles about methyl (phenyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 225640-45-9
methyl (phenyl 2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate

: 725228-92-2
methyl (phenyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate

Guidance literature:: With pyridine; at 20 ℃; for 3h;
DOI:10.1021/ol049380+

Reference yield:

: 231623-55-5
phenyl 2,3-di-O-benzyl-1-thio-β-D-galactopyranoside

: 725228-92-2
methyl (phenyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 2,2,6,6-tetramethyl-1-piperidinyloxyl; [bis(acetoxy)iodo]benzene / CH₂Cl₂; H₂O / 0.75 h / 20 °C

2: 93 percent / dimethylformamide; diethyl ether / 20 °C

3: 100 percent / pyridine / 3 h / 20 °C

With pyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol049380+

Reference yield:

: 725228-83-1
phenyl 2,3-di-O-benzyl-1-thio-β-D-galactopyranosiduronic acid

: 725228-92-2
methyl (phenyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-β-D-galactopyranosid)uronate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / dimethylformamide; diethyl ether / 20 °C

2: 100 percent / pyridine / 3 h / 20 °C

With pyridine; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ol049380+