chlorocyclohexylphosphine-pentacarbonyl-chromium⁽⁰⁾=Chlorocyclohexylphosphin-pentacarbonyl-chrom⁽⁰⁾

Base Information

• Chemical Name: chlorocyclohexylphosphine-pentacarbonyl-chromium⁽⁰⁾=Chlorocyclohexylphosphin-pentacarbonyl-chrom⁽⁰⁾
• CAS No.: 131413-37-1
• Molecular Formula: C₁₁H₁₂ClCrO₅P
• Molecular Weight: 342.636

Synonyms:chlorocyclohexylphosphine-pentacarbonyl-chromium⁽⁰⁾=Chlorocyclohexylphosphin-pentacarbonyl-chrom⁽⁰⁾

Chemical Property of chlorocyclohexylphosphine-pentacarbonyl-chromium⁽⁰⁾=Chlorocyclohexylphosphin-pentacarbonyl-chrom⁽⁰⁾

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Technology Process of chlorocyclohexylphosphine-pentacarbonyl-chromium⁽⁰⁾=Chlorocyclohexylphosphin-pentacarbonyl-chrom⁽⁰⁾

There total 1 articles about chlorocyclohexylphosphine-pentacarbonyl-chromium⁽⁰⁾=Chlorocyclohexylphosphin-pentacarbonyl-chrom⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

diethylaminocyclohexylphosphine-pentacarbonyl-chromium(0)=Diethylaminocyclohexylphosphin-pentacarbonyl-chrom(0) (131441-43-5) → chlorocyclohexylphosphine-pentacarbonyl-chromium(0)=Chlorocyclohexylphosphin-pentacarbonyl-chrom(0) (131413-37-1)

Guidance literature:

With hydrogenchloride; In pentane; byproducts: Et2NH*HCl; (Ar); addn. of gaseous HCl under stirring at o°C; removal of solvent in vac. at room temp.; digered with pentane; filtn.; dried in vac.; chromy. (silica gel/pentane); elem. anal.; IR; (31)P NMR; mass spectra;

DOI:10.1016/0022-328X(90)85169-Y

upstream raw materials:

diethylaminocyclohexylphosphine-pentacarbonyl-chromium⁽⁰⁾=Diethylaminocyclohexylphosphin-pentacarbonyl-chrom⁽⁰⁾

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