C₅₄H₇₆O₈Si₂

Base Information

Chemical Name:C₅₄H₇₆O₈Si₂
CAS No.:1391927-59-5
Molecular Formula:C₅₄H₇₆O₈Si₂
Molecular Weight:909.364
Hs Code.:

C<sub>54</sub>H<sub>76</sub>O<sub>8</sub>Si<sub>2</sub>

Synonyms:C₅₄H₇₆O₈Si₂

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Chemical Property of C₅₄H₇₆O₈Si₂

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Technology Process of C₅₄H₇₆O₈Si₂

There total 13 articles about C₅₄H₇₆O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S)-4-benzyloxy-2-(4-methoxybenzyloxy)-butyraldehyde

: C₃₈H₆₂O₄Si₃

: 1391927-59-5
C₅₄H₇₆O₈Si₂

Guidance literature:: With magnesium bromide diethyl etherate; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1021/ol301795a

Reference yield:

: 92512-41-9
C₂₁H₂₈O₃Si

: 1391927-59-5
C₅₄H₇₆O₈Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 - -55 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

2.3: 0.33 h / -78 °C / Inert atmosphere

3.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 5 h / 20 °C / Inert atmosphere

4.1: pyridinium p-toluenesulfonate / methanol / 22 h / 40 °C / Inert atmosphere

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

6.1: tetrahydrofuran / -78 °C / Inert atmosphere

6.2: 1 h / 20 °C / Molecular sieve; Inert atmosphere

7.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 °C

8.1: 1H-imidazole; dmap / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

9.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.67 h / -78 °C / Inert atmosphere

9.2: 0.83 h / -78 °C / Inert atmosphere

10.1: magnesium bromide diethyl etherate / dichloromethane / -78 - 0 °C / Inert atmosphere

With 1H-imidazole; dmap; n-butyllithium; tetrapropylammonium perruthennate; magnesium bromide diethyl etherate; water; pyridinium p-toluenesulfonate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; potassium hexamethylsilazane; sodium hydride; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene;
DOI:10.1021/ol301795a

Reference yield:

: 1391927-58-4
C₃₅H₅₄O₄Si₂

: 1391927-59-5
C₅₄H₇₆O₈Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.67 h / -78 °C / Inert atmosphere

1.2: 0.83 h / -78 °C / Inert atmosphere

2.1: magnesium bromide diethyl etherate / dichloromethane / -78 - 0 °C / Inert atmosphere

With magnesium bromide diethyl etherate; potassium hexamethylsilazane; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ol301795a