(S)-5-(2,2-dimethyl-6-methylenecyclohexylmethylsulfinyl)-1-phenyl-1H-tetrazole

Base Information

Chemical Name:(S)-5-(2,2-dimethyl-6-methylenecyclohexylmethylsulfinyl)-1-phenyl-1H-tetrazole
CAS No.:782474-35-5
Molecular Formula:C₁₇H₂₂N₄OS
Molecular Weight:330.454
Hs Code.:

Synonyms:(S)-5-(2,2-dimethyl-6-methylenecyclohexylmethylsulfinyl)-1-phenyl-1H-tetrazole

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Chemical Property of (S)-5-(2,2-dimethyl-6-methylenecyclohexylmethylsulfinyl)-1-phenyl-1H-tetrazole

Chemical Property:

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Technology Process of (S)-5-(2,2-dimethyl-6-methylenecyclohexylmethylsulfinyl)-1-phenyl-1H-tetrazole

There total 3 articles about (S)-5-(2,2-dimethyl-6-methylenecyclohexylmethylsulfinyl)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: (S)-5-(2,2-dimethyl-6-methylenecyclohexylmethylsulfanyl)-1-phenyl-1H-tetrazole

: 782474-35-5
(S)-5-(2,2-dimethyl-6-methylenecyclohexylmethylsulfinyl)-1-phenyl-1H-tetrazole

: (S)-5-(2,2-dimethyl-6-methylenecyclohexylmethylsulfanyl)-1-phenyl-1H-tetrazole

Guidance literature:: With ammonium molybdate tetrahydrate; dihydrogen peroxide; In ethanol; at 20 ℃;
DOI:10.1021/ja048084p

Reference yield:

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 782474-35-5
(S)-5-(2,2-dimethyl-6-methylenecyclohexylmethylsulfinyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / triphenylphosphite; diisopropylazodicarboxylate / tetrahydrofuran / 3 h / 20 °C

2: 32 percent / aq. H₂O₂; ammonium heptamolybdate tetrahydrate / ethanol / 20 °C

With triphenyl phosphite; ammonium molybdate tetrahydrate; di-isopropyl azodicarboxylate; dihydrogen peroxide; In tetrahydrofuran; ethanol; 1: Mitsunobu reaction;
DOI:10.1021/ja048084p

Reference yield:

: 166022-29-3
(S)-(+)-(2',2'-dimethyl-6'-methylene-1'-cyclohexyl)methanol

: 782474-35-5
(S)-5-(2,2-dimethyl-6-methylenecyclohexylmethylsulfinyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / triphenylphosphite; diisopropylazodicarboxylate / tetrahydrofuran / 3 h / 20 °C

2: 32 percent / aq. H₂O₂; ammonium heptamolybdate tetrahydrate / ethanol / 20 °C

With triphenyl phosphite; ammonium molybdate tetrahydrate; di-isopropyl azodicarboxylate; dihydrogen peroxide; In tetrahydrofuran; ethanol; 1: Mitsunobu reaction;
DOI:10.1021/ja048084p