C₃₉H₆₄O₄Si₂

Base Information

Chemical Name:C₃₉H₆₄O₄Si₂
CAS No.:1404304-78-4
Molecular Formula:C₃₉H₆₄O₄Si₂
Molecular Weight:653.106
Hs Code.:

C<sub>39</sub>H<sub>64</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₉H₆₄O₄Si₂

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Chemical Property of C₃₉H₆₄O₄Si₂

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Technology Process of C₃₉H₆₄O₄Si₂

There total 12 articles about C₃₉H₆₄O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1404304-81-9
C₃₉H₆₆O₄Si₂

: 1404304-78-4
C₃₉H₆₄O₄Si₂

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol302409g

Reference yield:

: 102517-37-3
(2R,3R)-1,2-epoxy-3-heptanol

: 1404304-78-4
C₃₉H₆₄O₄Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: 1H-imidazole / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

2.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 1 h / -78 - 20 °C / Inert atmosphere

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 6 h / 40 °C / Inert atmosphere

4.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl) / tetrahydrofuran / 50 °C / Inert atmosphere

5.1: triethylamine / methanol / 0.75 h / 20 °C / Inert atmosphere

6.1: magnesium bromide / diethyl ether / 16 h / 0 - 20 °C / Inert atmosphere

7.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C / Inert atmosphere

8.1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

8.2: 1 h / 0 °C / Inert atmosphere

9.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-dimethylpyridine; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; copper(l) iodide; dimethylsulfide borane complex; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; magnesium bromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1021/ol302409g

Reference yield:

: 1404304-64-8
C₂₃H₃₂O₂Si

: 1404304-78-4
C₃₉H₆₄O₄Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 1 h / -78 - 20 °C / Inert atmosphere

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 6 h / 40 °C / Inert atmosphere

3.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl) / tetrahydrofuran / 50 °C / Inert atmosphere

4.1: triethylamine / methanol / 0.75 h / 20 °C / Inert atmosphere

5.1: magnesium bromide / diethyl ether / 16 h / 0 - 20 °C / Inert atmosphere

6.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C / Inert atmosphere

7.1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

7.2: 1 h / 0 °C / Inert atmosphere

8.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-dimethylpyridine; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; copper(l) iodide; dimethylsulfide borane complex; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; magnesium bromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1021/ol302409g