Cyclohexanecarbonyl-((1S,2R)-1,2-dimethoxy-2-phenyl-ethyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

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Chemical Name:Cyclohexanecarbonyl-((1S,2R)-1,2-dimethoxy-2-phenyl-ethyl)-carbamic acid 2-trimethylsilanyl-ethyl ester
CAS No.:204579-13-5
Molecular Formula:C₂₃H₃₇NO₅Si
Molecular Weight:435.636
Hs Code.:

Synonyms:Cyclohexanecarbonyl-((1S,2R)-1,2-dimethoxy-2-phenyl-ethyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

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Chemical Property of Cyclohexanecarbonyl-((1S,2R)-1,2-dimethoxy-2-phenyl-ethyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

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Technology Process of Cyclohexanecarbonyl-((1S,2R)-1,2-dimethoxy-2-phenyl-ethyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

There total 6 articles about Cyclohexanecarbonyl-((1S,2R)-1,2-dimethoxy-2-phenyl-ethyl)-carbamic acid 2-trimethylsilanyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 204579-13-5
Cyclohexanecarbonyl-((1S,2R)-1,2-dimethoxy-2-phenyl-ethyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / (PhO)2PON₃, Et₃N / tetrahydrofuran

2: 1) LHMDS, 2) DMAP / 1) THF, -78 deg C, 2) THF, -78 deg C, 30 min

With dmap; diphenyl phosphoryl azide; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1021/jo980024c

Reference yield:

: 204578-99-4
(2S,3R)-2,3-Dimethoxy-3-phenyl-propionic acid

: 204579-13-5
Cyclohexanecarbonyl-((1S,2R)-1,2-dimethoxy-2-phenyl-ethyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / (PhO)2PON₃, Et₃N / tetrahydrofuran

2: 1) LHMDS, 2) DMAP / 1) THF, -78 deg C, 2) THF, -78 deg C, 30 min

With dmap; diphenyl phosphoryl azide; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1021/jo980024c

Reference yield:

: 1027419-66-4
(2S,3R)-2,3-Dimethoxy-3-phenyl-propionic acid methyl ester

: 204579-13-5
Cyclohexanecarbonyl-((1S,2R)-1,2-dimethoxy-2-phenyl-ethyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / tetrahydrofuran; H₂O

2: 75 percent / (PhO)2PON₃, Et₃N / tetrahydrofuran

3: 1) LHMDS, 2) DMAP / 1) THF, -78 deg C, 2) THF, -78 deg C, 30 min

With dmap; sodium hydroxide; diphenyl phosphoryl azide; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; water;
DOI:10.1021/jo980024c