(R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-ornithinamide

Base Information

• Chemical Name: (R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-ornithinamide
• CAS No.: 191871-42-8
• Molecular Formula: C₂₁H₂₅Cl₂N₅O₃
• Molecular Weight: 466.367

Synonyms:(R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-ornithinamide

Chemical Property of (R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-ornithinamide

Chemical Property:

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Technology Process of (R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-ornithinamide

There total 6 articles about (R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-ornithinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N2-[[(3,4-dichlorophenyl)amino]carbonyl]-N5-(phenylmethoxycarbonyl)-ornithinamide → (R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N2-[[(3,4-dichlorophenyl)amino]carbonyl]-ornithinamide (191871-42-8)

Guidance literature:

With hydrogen bromide; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; acetic acid; ethyl acetate;

Reference yield:

4-cyanophenylacetic acid (5462-71-5) → (R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N2-[[(3,4-dichlorophenyl)amino]carbonyl]-ornithinamide (191871-42-8)

Guidance literature:

Multi-step reaction with 4 steps

1: ammonia; 1,1'-carbonyldiimidazole / tetrahydrofuran; ethyl acetate

2: aluminum nickel / methanol; hydrogen

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate

4: hydrogen bromide / (2S)-N-methyl-1-phenylpropan-2-amine hydrate; acetic acid; ethyl acetate

With ammonia; hydrogen bromide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,1'-carbonyldiimidazole; aluminum nickel; In tetrahydrofuran; methanol; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; hydrogen; acetic acid; ethyl acetate;

Reference yield:

2-(4-cyanophenyl)acetamide (117753-06-7) → (R,S)-N-[[4-(aminocarbonylmethyl)phenyl]methyl]-N2-[[(3,4-dichlorophenyl)amino]carbonyl]-ornithinamide (191871-42-8)

Guidance literature:

Multi-step reaction with 3 steps

1: aluminum nickel / methanol; hydrogen

2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate

3: hydrogen bromide / (2S)-N-methyl-1-phenylpropan-2-amine hydrate; acetic acid; ethyl acetate

With hydrogen bromide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; aluminum nickel; In methanol; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; hydrogen; acetic acid; ethyl acetate;

upstream raw materials:

2-[4-(aminomethyl)phenyl]acetamide

1-(3,4-dichlorophenyl)-4-[3-[(phenylmethoxycarbonyl)amino]propyl]-imidazolidin-2,5-dione

(R,S)-N₂-[[(3,4-dichlorophenyl)amino]carbonyl]-N₅-(phenylmethoxycarbonyl)-ornithine

4-cyanophenylacetic acid

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