1-Phenyl-1,4,6,7,8,9-hexahydropyrazolo<3',4':4,5>pyrimido<2,1-c><1,2,4>triazin-7-one

Base Information

Chemical Name:1-Phenyl-1,4,6,7,8,9-hexahydropyrazolo<3',4':4,5>pyrimido<2,1-c><1,2,4>triazin-7-one
CAS No.:130024-11-2
Molecular Formula:C₁₃H₁₂N₆O
Molecular Weight:268.278
Hs Code.:

Synonyms:1-Phenyl-1,4,6,7,8,9-hexahydropyrazolo<3',4':4,5>pyrimido<2,1-c><1,2,4>triazin-7-one

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Chemical Property of 1-Phenyl-1,4,6,7,8,9-hexahydropyrazolo<3',4':4,5>pyrimido<2,1-c><1,2,4>triazin-7-one

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Technology Process of 1-Phenyl-1,4,6,7,8,9-hexahydropyrazolo<3',4':4,5>pyrimido<2,1-c><1,2,4>triazin-7-one

There total 3 articles about 1-Phenyl-1,4,6,7,8,9-hexahydropyrazolo<3',4':4,5>pyrimido<2,1-c><1,2,4>triazin-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 130024-08-7
Ethyl 6-chloro-1-phenyl-4,5-dihydro-1H-pyrazolo<3,4-d>pyrimidine-5-acetate

: 130024-11-2
1-Phenyl-1,4,6,7,8,9-hexahydropyrazolo<3',4':4,5>pyrimido<2,1-c><1,2,4>triazin-7-one

Guidance literature:: With hydrazine hydrate; In ethanol; Ambient temperature;
DOI:10.1002/jhet.5570270401

Reference yield:

: 99971-84-3
4,6-dichloro-1-phenyl-1H-pyrazolo<3,4-d>pyrimidine

: 130024-11-2
1-Phenyl-1,4,6,7,8,9-hexahydropyrazolo<3',4':4,5>pyrimido<2,1-c><1,2,4>triazin-7-one

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / NaBH₄ / ethanol; CHCl₃ / Ambient temperature

2: 64 percent / 10N aq. NaOH, Bu₄NI / CH₂Cl₂ / 3 h / Ambient temperature

3: 90 percent / N₂H₄*H₂O / ethanol / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; hydrazine hydrate; In ethanol; dichloromethane; chloroform;
DOI:10.1002/jhet.5570270401

Reference yield:

: 130024-05-4
6-Chloro-1-phenyl-4,5-dihydro-1H-pyrazolo<3,4-d>pyrimidine

: 130024-11-2
1-Phenyl-1,4,6,7,8,9-hexahydropyrazolo<3',4':4,5>pyrimido<2,1-c><1,2,4>triazin-7-one

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / 10N aq. NaOH, Bu₄NI / CH₂Cl₂ / 3 h / Ambient temperature

2: 90 percent / N₂H₄*H₂O / ethanol / Ambient temperature

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; hydrazine hydrate; In ethanol; dichloromethane;
DOI:10.1002/jhet.5570270401