4-methyl-N-(4-methyl-penta-2,3-dienyl)-N-(3-naphthalen-2-yl-prop-2-ynyl)-benzenesulfonamide

Base Information

• Chemical Name: 4-methyl-N-(4-methyl-penta-2,3-dienyl)-N-(3-naphthalen-2-yl-prop-2-ynyl)-benzenesulfonamide
• CAS No.: 885702-89-6
• Molecular Formula: C₂₆H₂₅NO₂S
• Molecular Weight: 415.556

Synonyms:4-methyl-N-(4-methyl-penta-2,3-dienyl)-N-(3-naphthalen-2-yl-prop-2-ynyl)-benzenesulfonamide

Chemical Property of 4-methyl-N-(4-methyl-penta-2,3-dienyl)-N-(3-naphthalen-2-yl-prop-2-ynyl)-benzenesulfonamide

Chemical Property:

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Technology Process of 4-methyl-N-(4-methyl-penta-2,3-dienyl)-N-(3-naphthalen-2-yl-prop-2-ynyl)-benzenesulfonamide

There total 1 articles about 4-methyl-N-(4-methyl-penta-2,3-dienyl)-N-(3-naphthalen-2-yl-prop-2-ynyl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-N-(3-naphthalen-2-yl-prop-2-ynyl)-benzenesulfonamide + 4-methylpenta-2,3-dien-1-ol (2425-45-8) → 4-methyl-N-(4-methyl-penta-2,3-dienyl)-N-(3-naphthalen-2-yl-prop-2-ynyl)-benzenesulfonamide (885702-89-6)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

DOI:10.1002/hlca.200690165

Reference yield: 91.0%

4-methyl-N-(4-methyl-penta-2,3-dienyl)-N-(3-naphthalen-2-yl-prop-2-ynyl)-benzenesulfonamide (885702-89-6) + trifluorormethanesulfonic acid (1493-13-6) → 11,11-dimethyl-2-tosyl-1,2,3,11,12,12a-hexahydronaphtho-[2′,3′:4,5]cyclohepta[1,2-c]pyrrol-4-yl trifluoromethanesulfonate

Guidance literature:

In 1,2-dichloro-ethane; at 20 ℃; for 24h;

DOI:10.1021/acs.joc.8b00393

Reference yield: 82.0%

4-methyl-N-(4-methyl-penta-2,3-dienyl)-N-(3-naphthalen-2-yl-prop-2-ynyl)-benzenesulfonamide (885702-89-6) → 6-isopropenyl-7-(2-naphthyl)-3-tosyl-3-azabicyclo[3.2.0]hept-6-ene

Guidance literature:

platinum(II) chloride; In toluene; at 80 ℃; for 12h;

DOI:10.1055/s-2006-932482

upstream raw materials:

4-methylpenta-2,3-dien-1-ol

Downstream raw materials:

(Z)-3-(2-methylprop-1-enyl)-4-(naphthalen-2-ylmethylene)-1-tosylpyrrolidine

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