Os{PCO(CF₃)}(CO)2(P(C₆H₅)3)2

Base Information

Chemical Name:Os{PCO(CF₃)}(CO)2(P(C₆H₅)3)2
CAS No.:103932-33-8
Molecular Formula:C₄₀H₃₀F₃O₃OsP₃
Molecular Weight:898.793
Hs Code.:

Os{PCO(CF<sub>3</sub>)}(CO)2(P(C<sub>6</sub>H<sub>5</sub>)3)2

Synonyms:Os{PCO(CF₃)}(CO)2(P(C₆H₅)3)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Os{PCO(CF₃)}(CO)2(P(C₆H₅)3)2

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Technology Process of Os{PCO(CF₃)}(CO)2(P(C₆H₅)3)2

There total 3 articles about Os{PCO(CF₃)}(CO)2(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 103932-34-9
OsCl{PHCO(CF₃)}(CO)2(P(C₆H₅)3)2

: 7646-69-7
sodium hydride

: 103932-33-8
Os{PCO(CF₃)}(CO)2(P(C₆H₅)3)2

Guidance literature:: In tetrahydrofuran; byproducts: hydrogen, NaCl; refluxed for 1.5 h; mixt. cooled; excess of NaH removed by filtration through Celite; washed with THF; THF removed in vacuo;; redissolved in CH2Cl2; addn. of ethanol; concentration; elem. anal.;
DOI:10.1016/0022-328X(88)80325-5

Reference yield: 81.0%

: 131077-15-1
osmium(η1-OC(O)Me){PH(C(O)CF3)}(CO)2(PPh3)2

: 7646-69-7
sodium hydride

: 103932-33-8
osmium(P=C(O)CF₃)(CO)2(PPh₃)2

Guidance literature:: In tetrahydrofuran; NaH as 45% dispersion in paraffin; stirring at room temp. for 1 h; filtration through Celite; removal of solvent in vac.; recrystd. from CH2Cl2/EtOH;
DOI:10.1016/0022-328X(90)80204-D

Reference yield:

: 103932-34-9
[OsCl(PHCOCF₃)(CO)2(P(C₆H₅)3)2]

: 103932-33-8
Os{PCO(CF₃)}(CO)2(P(C₆H₅)3)2

Guidance literature:: With NaH or 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; heated under reflux; elem. anal.;
DOI:10.1039/c39850001594