Technology Process of C48H56N4O8SSi
There total 13 articles about C48H56N4O8SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0);
In
toluene;
at 110 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / tetrahydrofuran / 16 h / 20 °C
2.1: triethylamine / dichloromethane / 20 °C
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
3.2: 20 °C
4.1: tetrakis(triphenylphosphine) palladium(0) / toluene / 110 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); sodium hydride; triethylamine;
In
tetrahydrofuran; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: sodium hydride / 1,4-dioxane / 0.25 h / 10 °C
1.2: 10 - 100 °C
2.1: sodium hydroxide; water / methanol / 4 h / 50 °C
3.1: potassium carbonate; silver(I) acetate; 1-methyl-pyrrolidin-2-one / 2 h / 110 °C
4.1: bromine; CH3COONa / acetic acid / 1 h / 20 °C
5.1: potassium carbonate / acetonitrile / 3 h / 20 °C
6.1: borane-THF / tetrahydrofuran / 8 h / 20 °C
7.1: carbon dioxide / methanol
8.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
8.2: 20 °C
9.1: tetrakis(triphenylphosphine) palladium(0) / toluene / 110 °C / Inert atmosphere
With
1-methyl-pyrrolidin-2-one; tetrakis(triphenylphosphine) palladium(0); borane-THF; carbon dioxide; CH3COONa; water; bromine; silver(I) acetate; sodium hydride; potassium carbonate; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; acetic acid; toluene; acetonitrile;