C₃₃H₄₁N₃O₇

Base Information

• Chemical Name: C₃₃H₄₁N₃O₇
• CAS No.: 937393-51-6
• Molecular Formula: C₃₃H₄₁N₃O₇
• Molecular Weight: 591.704
• Mol file: 937393-51-6.mol

Synonyms:C₃₃H₄₁N₃O₇

Chemical Property of C₃₃H₄₁N₃O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₄₁N₃O₇

There total 10 articles about C₃₃H₄₁N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Nα-2,3-dibenzyloxybenzoyl-Nδ-benzyloxycarbonyl-D-ornithinyl-L-serine tert-butyl ester (937393-48-1) → C33H41N3O7 (937393-51-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 3h;

DOI:10.1016/j.tetlet.2007.02.125

Reference yield:

Nα-2,3-dibenzyloxybenzoyl-Nδ-benzyloxycarbonyl-D-ornithine (937393-45-8) → C33H41N3O7 (937393-51-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / DBTU; TEA / dimethylformamide

2: 100 percent / H₂ / Pd/C / methanol / 3 h / 20 °C

With TEA; hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;

DOI:10.1016/j.tetlet.2007.02.125

Reference yield:

methyl-2,3-dihydroxybenzoate (2411-83-8) → C33H41N3O7 (937393-51-6)

Guidance literature:

Multi-step reaction with 5 steps

1: 99 percent / potassium carbonate / Heating

2: 100 percent / aq. barium hydroxide / tetrahydrofuran / 12 h / 50 °C

3: 79 percent / TBTU; Et₃N / dimethylformamide / 16 h / 20 °C

4: 81 percent / DBTU; TEA / dimethylformamide

5: 100 percent / H₂ / Pd/C / methanol / 3 h / 20 °C

With barium dihydroxide; TEA; hydrogen; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

DOI:10.1016/j.tetlet.2007.02.125

upstream raw materials:

Nα-2,3-dibenzyloxybenzoyl-Nδ-benzyloxycarbonyl-D-ornithinyl-L-serine tert-butyl ester

Nα-2,3-dibenzyloxybenzoyl-Nδ-benzyloxycarbonyl-D-ornithine

methyl-2,3-dihydroxybenzoate

acetic acid tert-butyl ester

Downstream raw materials:

C₄₄H₅₉N₅O₁₁