[(C₅H₅)(C₅H₄)Zr(P(CH₃)2C₆H₅)]2

Base Information

Chemical Name:[(C₅H₅)(C₅H₄)Zr(P(CH₃)2C₆H₅)]2
CAS No.:71844-81-0
Molecular Formula:C₃₆H₄₀P₂Zr₂
Molecular Weight:717.109
Hs Code.:

[(C<sub>5</sub>H<sub>5</sub>)(C<sub>5</sub>H<sub>4</sub>)Zr(P(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>)]2

Synonyms:[(C₅H₅)(C₅H₄)Zr(P(CH₃)2C₆H₅)]2

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Chemical Property of [(C₅H₅)(C₅H₄)Zr(P(CH₃)2C₆H₅)]2

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Technology Process of [(C₅H₅)(C₅H₄)Zr(P(CH₃)2C₆H₅)]2

There total 1 articles about [(C₅H₅)(C₅H₄)Zr(P(CH₃)2C₆H₅)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1291-32-3
zirconocene dichloride

: 672-66-2
Dimethyl(phenyl)phosphine

: 71844-81-0
[(C₅H₅)(C₅H₄)Zr(P(CH₃)2C₆H₅)]2

Guidance literature:: With sodium amalgam; In tetrahydrofuran; byproducts: H2; (Ar); complex soln. stirred at room temp. with Na#Hg for 24 h, decanted, filtered, kept for 24 h at room temp., P(CH3)2C6H5 added, heated for 60 h at 50-55°C; evapd., extd. with C6H6, concd., not isolated, detected by NMR;
DOI:10.1021/ic50216a033

Reference yield: 60.0%

: 71844-81-0
[(C₅H₅)(C₅H₄)Zr(P(CH₃)2C₆H₅)]2

: 1291-32-3
zirconocene dichloride

: 672-66-2
Dimethyl(phenyl)phosphine

Guidance literature:: With hydrogenchloride; In benzene-d6; (N2); HCl gas added to complex soln. at 0°C, shaken at room temp.; not isolated, detected by NMR;
DOI:10.1021/ic50216a033