tert-butyl (1S,2R,3R,αR)-2-[N-3,4-dimethoxybenzyl-N-(α-methylbenzyl)-amino]-3-isopropylcyclopentanecarboxylate

Base Information

Chemical Name:tert-butyl (1S,2R,3R,αR)-2-[N-3,4-dimethoxybenzyl-N-(α-methylbenzyl)-amino]-3-isopropylcyclopentanecarboxylate
CAS No.:1280736-77-7
Molecular Formula:C₃₀H₄₃NO₄
Molecular Weight:481.676
Hs Code.:

Synonyms:tert-butyl (1S,2R,3R,αR)-2-[N-3,4-dimethoxybenzyl-N-(α-methylbenzyl)-amino]-3-isopropylcyclopentanecarboxylate

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Chemical Property of tert-butyl (1S,2R,3R,αR)-2-[N-3,4-dimethoxybenzyl-N-(α-methylbenzyl)-amino]-3-isopropylcyclopentanecarboxylate

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Technology Process of tert-butyl (1S,2R,3R,αR)-2-[N-3,4-dimethoxybenzyl-N-(α-methylbenzyl)-amino]-3-isopropylcyclopentanecarboxylate

There total 1 articles about tert-butyl (1S,2R,3R,αR)-2-[N-3,4-dimethoxybenzyl-N-(α-methylbenzyl)-amino]-3-isopropylcyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 17480-69-2
(S)-N-benzyl-1-phenylethylamine

: 134430-93-6,308273-67-8,680185-65-3
(R)-N-(3,4-dimethoxybenzyl)-N-(α-methylbenzyl)amine

: 820236-12-2
tert-butyl (RS)-3-(1'-methylethyl)cyclopentene-1-carboxylate

: 820236-47-3
tert-butyl (1R,2S,3S,αS)-3-(1'-methylethyl)-2-(N-benzyl-N-α-methylbenzylamino)-cyclopentane-1-carboxylate

: tert-butyl (αR)-2-[N-3,4-dimethoxybenzyl-N-(α-methylbenzyl)-amino]-3-isopropylcyclopentanecarboxylate

: 1280736-77-7
tert-butyl (1S,2R,3R,αR)-2-[N-3,4-dimethoxybenzyl-N-(α-methylbenzyl)-amino]-3-isopropylcyclopentanecarboxylate

Guidance literature:: (S)-N-benzyl-1-phenylethylamine; (R)-N-(3,4-dimethoxybenzyl)-N-(α-methylbenzyl)amine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

tert-butyl (RS)-3-(1'-methylethyl)cyclopentene-1-carboxylate; In tetrahydrofuran; hexane; at -78 ℃; for 3h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; hexane; at -78 - 30 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tetasy.2010.12.007

Reference yield: 84.0%

: 1280736-77-7
tert-butyl (1S,2R,3R,αR)-2-[N-3,4-dimethoxybenzyl-N-(α-methylbenzyl)-amino]-3-isopropylcyclopentanecarboxylate

: 1280737-29-2
tert-butyl (R,R,R,R)-2-[N-benzyl-(N-α-methylbenzyl)-amino]-3-isopropylcyclopentane-1-carboxylate

Guidance literature:: With potassium tert-butylate; tert-butyl alcohol; for 8h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetasy.2010.12.007