N₄,N₇-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine

Base Information

• Chemical Name: N₄,N₇-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine
• CAS No.: 1154500-40-9
• Molecular Formula: C₅₉H₇₈N₆O₁₅
• Molecular Weight: 1111.3

Synonyms:N₄,N₇-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine

Chemical Property of N₄,N₇-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine

Chemical Property:

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Technology Process of N₄,N₇-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine

There total 1 articles about N₄,N₇-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N1-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N7-[4-(phthalimido)butyl]norspermidine (1154500-38-5) + N-tert-butoxycarbonyl-L-threonine N-hydroxysuccinimide ester (63076-44-8) → N4,N7-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N1-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N7-[4-(phthalimido)butyl]norspermidine (1154500-40-9)

Guidance literature:

In N,N-dimethyl-formamide; at 40 ℃; for 72h;

DOI:10.1021/jm900119q

Reference yield: 90.0%

N4,N7-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N1-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N7-[4-(phthalimido)butyl]norspermidine (1154500-40-9) → N4,N8-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N1-[2,3-bis(4-methoxybenzyloxy)benzoyl]thermospermine (1154500-43-2)

Guidance literature:

With hydrazine hydrate; In ethanol; at 20 ℃; for 16h;

DOI:10.1021/jm900119q

upstream raw materials:

N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine

N-tert-butoxycarbonyl-L-threonine N-hydroxysuccinimide ester

Downstream raw materials:

N₄,N₈-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]thermospermine

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