(E)-2-(3-methyl-1-tosyl-1-azaspiro[4.5]decan-4-ylidene)-2-(triisopropylsilyl)acetonitrile

Base Information

Chemical Name:(E)-2-(3-methyl-1-tosyl-1-azaspiro[4.5]decan-4-ylidene)-2-(triisopropylsilyl)acetonitrile
CAS No.:1430722-85-2
Molecular Formula:C₂₈H₄₄N₂O₂SSi
Molecular Weight:500.821
Hs Code.:

Synonyms:(E)-2-(3-methyl-1-tosyl-1-azaspiro[4.5]decan-4-ylidene)-2-(triisopropylsilyl)acetonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(3-methyl-1-tosyl-1-azaspiro[4.5]decan-4-ylidene)-2-(triisopropylsilyl)acetonitrile

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Technology Process of (E)-2-(3-methyl-1-tosyl-1-azaspiro[4.5]decan-4-ylidene)-2-(triisopropylsilyl)acetonitrile

There total 2 articles about (E)-2-(3-methyl-1-tosyl-1-azaspiro[4.5]decan-4-ylidene)-2-(triisopropylsilyl)acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1430722-84-1
N-allyl-4-methyl-N-(1-((triisopropylsilyl)ethynyl)cyclohexyl)benzenesulfonamide

: 75-86-5
2-hydroxy-2-methylpropanenitrile

: 1430722-85-2
(E)-2-(3-methyl-1-tosyl-1-azaspiro[4.5]decan-4-ylidene)-2-(triisopropylsilyl)acetonitrile

Guidance literature:: With triphenyl phosphite; tetrakis(triphenylphosphite)nickel⁽⁰⁾; In toluene; at 150 ℃; for 24h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo400342y

Reference yield: 13.0%

: 1430722-84-1
N-allyl-4-methyl-N-(1-((triisopropylsilyl)ethynyl)cyclohexyl)benzenesulfonamide

: 75-86-5
2-hydroxy-2-methylpropanenitrile

: 50487-71-3
4-methyl-N-(2-propenyl)benzenesulfonamide

: 1430722-85-2
(E)-2-(3-methyl-1-tosyl-1-azaspiro[4.5]decan-4-ylidene)-2-(triisopropylsilyl)acetonitrile

: 1430722-86-3
(cyclohex-1-en-1-ylethynyl)triisopropylsilane

Guidance literature:: With triphenyl phosphite; tetrakis(triphenylphosphite)nickel⁽⁰⁾; In toluene; at 150 ℃; for 8h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo400342y