diethyl 1-[(cyclohexylidenemethyl)(methoxycarbonyl)amino]vinylphosphonate

Base Information

Chemical Name:diethyl 1-[(cyclohexylidenemethyl)(methoxycarbonyl)amino]vinylphosphonate
CAS No.:946603-38-9
Molecular Formula:C₁₅H₂₆NO₅P
Molecular Weight:331.349
Hs Code.:

Synonyms:diethyl 1-[(cyclohexylidenemethyl)(methoxycarbonyl)amino]vinylphosphonate

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Chemical Property of diethyl 1-[(cyclohexylidenemethyl)(methoxycarbonyl)amino]vinylphosphonate

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Technology Process of diethyl 1-[(cyclohexylidenemethyl)(methoxycarbonyl)amino]vinylphosphonate

There total 2 articles about diethyl 1-[(cyclohexylidenemethyl)(methoxycarbonyl)amino]vinylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 946603-27-6
diethyl 2-chloro-1-[(cyclohexylidenemethyl)(methoxycarbonyl)amino]ethylphosphonate

: 946603-38-9
diethyl 1-[(cyclohexylidenemethyl)(methoxycarbonyl)amino]vinylphosphonate

Guidance literature:: With ammonia; In methanol; toluene; at 120 ℃; for 8h;
DOI:10.1016/j.tet.2007.05.023

Reference yield:

: 226991-91-9
2-diethylphosphono-1-(cyclohexylidenemethyl)aziridine

: 946603-38-9
diethyl 1-[(cyclohexylidenemethyl)(methoxycarbonyl)amino]vinylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / CH₂Cl₂ / 24 h / 20 °C

2: 51 percent / NH₃ / toluene; methanol / 8 h / 120 °C

With ammonia; In methanol; dichloromethane; toluene;
DOI:10.1016/j.tet.2007.05.023

Reference yield: 44.0%

: 946603-38-9
diethyl 1-[(cyclohexylidenemethyl)(methoxycarbonyl)amino]vinylphosphonate

: 100-46-9
benzylamine

: diethyl 1-benzyl-3-(cyclohexylidenemethyl)-2-oxo-4-imidazolidinylphosphonate

Guidance literature:: diethyl 1-[(cyclohexylidenemethyl)(methoxycarbonyl)amino]vinylphosphonate; benzylamine; In methanol; for 336h; Heating;

With potassium carbonate; In methanol; for 2h; Further stages.; Heating;
DOI:10.1016/j.tet.2007.05.023