2-deoxy-4,5-dihydroxy-1-[5-phenyltetrazole]-D-alloheptitol-7-N-(leucyl)sulfamate

Base Information

Chemical Name:2-deoxy-4,5-dihydroxy-1-[5-phenyltetrazole]-D-alloheptitol-7-N-(leucyl)sulfamate
CAS No.:1416466-13-1
Molecular Formula:C₂₀H₃₀N₆O₇S
Molecular Weight:498.56
Hs Code.:

Synonyms:2-deoxy-4,5-dihydroxy-1-[5-phenyltetrazole]-D-alloheptitol-7-N-(leucyl)sulfamate

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Chemical Property of 2-deoxy-4,5-dihydroxy-1-[5-phenyltetrazole]-D-alloheptitol-7-N-(leucyl)sulfamate

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Technology Process of 2-deoxy-4,5-dihydroxy-1-[5-phenyltetrazole]-D-alloheptitol-7-N-(leucyl)sulfamate

There total 10 articles about 2-deoxy-4,5-dihydroxy-1-[5-phenyltetrazole]-D-alloheptitol-7-N-(leucyl)sulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1416466-09-5
C₂₈H₄₂N₆O₉S

: 1416466-13-1
2-deoxy-4,5-dihydroxy-1-[5-phenyltetrazole]-D-alloheptitol-7-N-(leucyl)sulfamate

Guidance literature:: With trifluoroacetic acid; In water; at 0 - 20 ℃; for 4h;
DOI:10.1002/cbic.201200174

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-Ribose

: 1416466-13-1
2-deoxy-4,5-dihydroxy-1-[5-phenyltetrazole]-D-alloheptitol-7-N-(leucyl)sulfamate

Guidance literature:: Multi-step reaction with 9 steps

1: sulfuric acid / acetone / 0.5 h / 20 °C / Inert atmosphere

2: pyridine / 16 h / 20 °C / Inert atmosphere

3: acetonitrile / 8 h / 95 °C / Inert atmosphere

4: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

5: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

6: acetic acid / diethyl ether / 10 h / 55 °C

7: ISOPROPYLAMIDE / 0.83 h / 0 - 20 °C / Inert atmosphere

8: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 6 h / 20 °C / Inert atmosphere

9: trifluoroacetic acid / water / 4 h / 0 - 20 °C

With pyridine; lithium aluminium tetrahydride; ISOPROPYLAMIDE; sulfuric acid; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1002/cbic.201200174

Reference yield:

: 150584-00-2
5-O-p-anisyldiphenylmethyl-2,3-O-isopropylidene-β-D-ribofuranose

: 1416466-13-1
2-deoxy-4,5-dihydroxy-1-[5-phenyltetrazole]-D-alloheptitol-7-N-(leucyl)sulfamate

Guidance literature:: Multi-step reaction with 7 steps

1: acetonitrile / 8 h / 95 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

4: acetic acid / diethyl ether / 10 h / 55 °C

5: ISOPROPYLAMIDE / 0.83 h / 0 - 20 °C / Inert atmosphere

6: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 6 h / 20 °C / Inert atmosphere

7: trifluoroacetic acid / water / 4 h / 0 - 20 °C

With lithium aluminium tetrahydride; ISOPROPYLAMIDE; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cbic.201200174