2,3,4,5,6-pentafluoro-N-((Z)-6,7,8,9-tetrafluoro-2-methyl-1H-benzo[b]azepine-4(5H)-ylidene)benzol amine

Base Information

• Chemical Name: 2,3,4,5,6-pentafluoro-N-((Z)-6,7,8,9-tetrafluoro-2-methyl-1H-benzo[b]azepine-4(5H)-ylidene)benzol amine
• CAS No.: 1616064-09-5
• Molecular Formula: C₁₇H₇F₉N₂
• Molecular Weight: 410.242

Synonyms:2,3,4,5,6-pentafluoro-N-((Z)-6,7,8,9-tetrafluoro-2-methyl-1H-benzo[b]azepine-4(5H)-ylidene)benzol amine

Chemical Property of 2,3,4,5,6-pentafluoro-N-((Z)-6,7,8,9-tetrafluoro-2-methyl-1H-benzo[b]azepine-4(5H)-ylidene)benzol amine

Chemical Property:

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Technology Process of 2,3,4,5,6-pentafluoro-N-((Z)-6,7,8,9-tetrafluoro-2-methyl-1H-benzo[b]azepine-4(5H)-ylidene)benzol amine

There total 3 articles about 2,3,4,5,6-pentafluoro-N-((Z)-6,7,8,9-tetrafluoro-2-methyl-1H-benzo[b]azepine-4(5H)-ylidene)benzol amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

di(rhodium)tetracarbonyl dichloride + C17H8F10N2 (888314-93-0) → 2,3,4,5,6-pentafluoro-N-((Z)-6,7,8,9-tetrafluoro-2-methyl-1H-benzo[b]azepine-4(5H)-ylidene)benzol amine (1616064-09-5) + [Rh{κ2-(N,N)-(C6F5)NC(Me)CHC(Me)N(C6F5)}(CO)2] (1616063-95-6)

Guidance literature:

C₁₇H₈F₁₀N₂; With potassium hydride; In tetrahydrofuran; at -30 - 20 ℃; for 2h; Inert atmosphere;

di(rhodium)tetracarbonyl dichloride; In tetrahydrofuran; at -70 - 20 ℃; for 15h; Inert atmosphere;

DOI:10.1002/ejic.201402087

Reference yield:

[Rh{κ2-(N,N)-(C6F5)NC(Me)CHC(Me)N(C6F5)}(CO)2] (1616063-95-6) → 2,3,4,5,6-pentafluoro-N-((Z)-6,7,8,9-tetrafluoro-2-methyl-1H-benzo[b]azepine-4(5H)-ylidene)benzol amine (1616064-09-5)

Guidance literature:

In dichloromethane; at -30 ℃; for 72h; Inert atmosphere;

DOI:10.1002/ejic.201402087

Reference yield:

C17H8F10N2 (888314-93-0) → 2,3,4,5,6-pentafluoro-N-((Z)-6,7,8,9-tetrafluoro-2-methyl-1H-benzo[b]azepine-4(5H)-ylidene)benzol amine (1616064-09-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium hydride / tetrahydrofuran / 2 h / -30 - 20 °C / Inert atmosphere

1.2: polytetrafluoroethylene / 15 h / -70 - 20 °C / Inert atmosphere

2.1: dichloromethane / 72 h / -30 °C / Inert atmosphere

With potassium hydride; In tetrahydrofuran; dichloromethane;

DOI:10.1002/ejic.201402087

upstream raw materials:

C₁₇H₈F₁₀N₂

[Rh{κ²-(N,N)-(C₆F₅)NC(Me)CHC(Me)N(C₆F₅)}(CO)₂]

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