(E)-4,4,5,5-tetramethyl-2-(2-(2,6,6-trimethylcyclohex-1-enyl)-vinyl)-1,3,2-dioxaborolane

Base Information

Chemical Name:(E)-4,4,5,5-tetramethyl-2-(2-(2,6,6-trimethylcyclohex-1-enyl)-vinyl)-1,3,2-dioxaborolane
CAS No.:256518-16-8
Molecular Formula:C₁₇H₂₉BO₂
Molecular Weight:276.227
Hs Code.:

Synonyms:(E)-4,4,5,5-tetramethyl-2-(2-(2,6,6-trimethylcyclohex-1-enyl)-vinyl)-1,3,2-dioxaborolane

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Chemical Property of (E)-4,4,5,5-tetramethyl-2-(2-(2,6,6-trimethylcyclohex-1-enyl)-vinyl)-1,3,2-dioxaborolane

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Technology Process of (E)-4,4,5,5-tetramethyl-2-(2-(2,6,6-trimethylcyclohex-1-enyl)-vinyl)-1,3,2-dioxaborolane

There total 3 articles about (E)-4,4,5,5-tetramethyl-2-(2-(2,6,6-trimethylcyclohex-1-enyl)-vinyl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: C₁₆H₂₄BNO₄

: 256518-16-8
(E)-4,4,5,5-tetramethyl-2-(2-(2,6,6-trimethylcyclohex-1-enyl)-vinyl)-1,3,2-dioxaborolane

Guidance literature:: With sodium hydrogencarbonate; In methanol;
DOI:10.1038/nchem.1947

Reference yield: 25.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1892-05-3
2-ethynyl-1,3,3-trimethyl-1-cyclohexene

: 256518-16-8
(E)-4,4,5,5-tetramethyl-2-(2-(2,6,6-trimethylcyclohex-1-enyl)-vinyl)-1,3,2-dioxaborolane

Guidance literature:: With dimethylsulfide borane complex; In dichloromethane; at 0 - 50 ℃;
DOI:10.1016/S0040-4020(99)00962-X

Reference yield:

: 432-25-7
2,6,6-trimethylcyclohex-1-enecarbaldehyde

: 256518-16-8
(E)-4,4,5,5-tetramethyl-2-(2-(2,6,6-trimethylcyclohex-1-enyl)-vinyl)-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / LDA / tetrahydrofuran / -78 - 25 °C

2: 25 percent / BH₃*SMe₂ / CH₂Cl₂ / 0 - 50 °C

With dimethylsulfide borane complex; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; 1: Condensation / 2: hydroboration;
DOI:10.1016/S0040-4020(99)00962-X