(1E,2S,6R) dimethyl 2-(-6-(4-methoxyphenyl)tetrahydro-2H-pyran-2-yl)vinylphosphonate

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Chemical Name:(1E,2S,6R) dimethyl 2-(-6-(4-methoxyphenyl)tetrahydro-2H-pyran-2-yl)vinylphosphonate
CAS No.:1172595-00-4
Molecular Formula:C₁₆H₂₃O₅P
Molecular Weight:326.329
Hs Code.:

Synonyms:(1E,2S,6R) dimethyl 2-(-6-(4-methoxyphenyl)tetrahydro-2H-pyran-2-yl)vinylphosphonate

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Chemical Property of (1E,2S,6R) dimethyl 2-(-6-(4-methoxyphenyl)tetrahydro-2H-pyran-2-yl)vinylphosphonate

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Technology Process of (1E,2S,6R) dimethyl 2-(-6-(4-methoxyphenyl)tetrahydro-2H-pyran-2-yl)vinylphosphonate

There total 1 articles about (1E,2S,6R) dimethyl 2-(-6-(4-methoxyphenyl)tetrahydro-2H-pyran-2-yl)vinylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1172595-01-5
(2E,7R,1R) dimethyl [7-hydroxy-1-(methoxycarbonyloxy)-7-(4-methoxyphenyl)-hept-2-enyl]phosphonate

: 1172595-00-4
(1E,2S,6R) dimethyl 2-(-6-(4-methoxyphenyl)tetrahydro-2H-pyran-2-yl)vinylphosphonate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 60 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol900980s

Reference yield: 77.0%

: 1172595-00-4
(1E,2S,6R) dimethyl 2-(-6-(4-methoxyphenyl)tetrahydro-2H-pyran-2-yl)vinylphosphonate

: 1172595-02-6
(2S,6R) 6-(4-methoxyphenyl)tetrahydro-2H-pyran-2-carboxaldehyde

Guidance literature:: (1E,2S,6R) dimethyl 2-(-6-(4-methoxyphenyl)tetrahydro-2H-pyran-2-yl)vinylphosphonate; With ozone; In methanol; dichloromethane; at -78 ℃; for 0.5h;

With dimethylsulfide; In methanol; dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol900980s