Morpholino(N-phenyl-thiocarbonimidsaeure)-S-(2-benzoylvinyl)ester

Base Information

• Chemical Name: Morpholino(N-phenyl-thiocarbonimidsaeure)-S-(2-benzoylvinyl)ester
• CAS No.: 83241-69-4
• Molecular Formula: C₂₀H₂₀N₂O₂S
• Molecular Weight: 352.457
• Mol file: 83241-69-4.mol

Synonyms:Morpholino(N-phenyl-thiocarbonimidsaeure)-S-(2-benzoylvinyl)ester

Chemical Property of Morpholino(N-phenyl-thiocarbonimidsaeure)-S-(2-benzoylvinyl)ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Morpholino(N-phenyl-thiocarbonimidsaeure)-S-(2-benzoylvinyl)ester

There total 1 articles about Morpholino(N-phenyl-thiocarbonimidsaeure)-S-(2-benzoylvinyl)ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

N-Phenyl-morpholine-4-carboximidothioic acid (Z)-3-oxo-3-phenyl-propenyl ester; compound with perchloric acid (83241-70-7) → Morpholino(N-phenyl-thiocarbonimidsaeure)-S-(2-benzoylvinyl)ester (83241-69-4)

Guidance literature:

With potassium carbonate; In acetone;

DOI:10.1016/0040-4020(82)85072-2

Reference yield: 100.0%

Morpholino(N-phenyl-thiocarbonimidsaeure)-S-(2-benzoylvinyl)ester (83241-69-4) → Morpholine-4-carbothioic acid ((E)-3-oxo-3-phenyl-propenyl)-phenyl-amide (83241-90-1)

Guidance literature:

In toluene; for 1.5h; Heating;

DOI:10.1016/0040-4020(82)85072-2

Reference yield:

Morpholino(N-phenyl-thiocarbonimidsaeure)-S-(2-benzoylvinyl)ester (83241-69-4) → Morpholine-4-carbothioic acid ((Z)-3-oxo-3-phenyl-propenyl)-phenyl-amide (344582-49-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / toluene / 1.5 h / Heating

2: acetone-d6 / 5 h / Irradiation

In acetone; toluene;

DOI:10.1016/0040-4020(82)85072-2

upstream raw materials:

N-Phenyl-morpholine-4-carboximidothioic acid (Z)-3-oxo-3-phenyl-propenyl ester; compound with perchloric acid

Downstream raw materials:

Morpholinothiocarbonsaeure-N-phenyl>amid

Morpholine-4-carbothioic acid ((E)-3-oxo-3-phenyl-propenyl)-phenyl-amide

Morpholine-4-carbothioic acid ((Z)-3-oxo-3-phenyl-propenyl)-phenyl-amide