N-(3-aminopropyl)-N'-(6-{[6-(3-aminopropylamino)hexyl]benzylamino}hexyl)-N'-benzylhexane-1,6-diamine

Base Information

Chemical Name:N-(3-aminopropyl)-N'-(6-{[6-(3-aminopropylamino)hexyl]benzylamino}hexyl)-N'-benzylhexane-1,6-diamine
CAS No.:428879-84-9
Molecular Formula:C₃₈H₆₈N₆
Molecular Weight:608.998
Hs Code.:

Synonyms:N-(3-aminopropyl)-N'-(6-{[6-(3-aminopropylamino)hexyl]benzylamino}hexyl)-N'-benzylhexane-1,6-diamine

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Chemical Property of N-(3-aminopropyl)-N'-(6-{[6-(3-aminopropylamino)hexyl]benzylamino}hexyl)-N'-benzylhexane-1,6-diamine

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Technology Process of N-(3-aminopropyl)-N'-(6-{[6-(3-aminopropylamino)hexyl]benzylamino}hexyl)-N'-benzylhexane-1,6-diamine

There total 6 articles about N-(3-aminopropyl)-N'-(6-{[6-(3-aminopropylamino)hexyl]benzylamino}hexyl)-N'-benzylhexane-1,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 428879-83-8
3-{6-[benzyl-(6-{benzyl-[6-(2-cyanoethylamino)hexyl]amino}hexyl)amino]hexylamino}propionitrile

: 428879-84-9
N-(3-aminopropyl)-N'-(6-{[6-(3-aminopropylamino)hexyl]benzylamino}hexyl)-N'-benzylhexane-1,6-diamine

Guidance literature:: With sodium hydroxide; hydrogen; nickel; In ethanol; at 20 ℃; for 6h; under 775.743 Torr;
DOI:10.1021/jm011067f

Reference yield:

: 1947-00-8
6-(benzyloxycarbonylamino)hexanoic acid

: 428879-84-9
N-(3-aminopropyl)-N'-(6-{[6-(3-aminopropylamino)hexyl]benzylamino}hexyl)-N'-benzylhexane-1,6-diamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethyl chlorocarbonate; Et₃N / dioxane / 0.5 h

1.2: 70 percent / dioxane / 20 °C

2.1: 90 percent / 30percent HBr; AcOH; CF₃COOH / 2 h

3.1: 40 percent / 10 M BH₃*MeSMe / bis-(2-methoxy-ethyl) ether / 10 h / 120 °C

4.1: 30 percent / methanol / 3 h / 0 °C

5.1: 90 percent / H₂; aq. NaOH / Raney Ni / ethanol / 6 h / 20 °C / 775.74 Torr

With sodium hydroxide; dimethylsulfide borane complex; hydrogen; chloroformic acid ethyl ester; acetic acid; triethylamine; trifluoroacetic acid; nickel; In 1,4-dioxane; methanol; ethanol; diethylene glycol dimethyl ether;
DOI:10.1021/jm011067f

Reference yield:

: 30070-99-6
N,N'-dibenzyl-1,6-diaminohexane

: 428879-84-9
N-(3-aminopropyl)-N'-(6-{[6-(3-aminopropylamino)hexyl]benzylamino}hexyl)-N'-benzylhexane-1,6-diamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethyl chlorocarbonate; Et₃N / dioxane / 0.5 h

1.2: 70 percent / dioxane / 20 °C

2.1: 90 percent / 30percent HBr; AcOH; CF₃COOH / 2 h

3.1: 40 percent / 10 M BH₃*MeSMe / bis-(2-methoxy-ethyl) ether / 10 h / 120 °C

4.1: 30 percent / methanol / 3 h / 0 °C

5.1: 90 percent / H₂; aq. NaOH / Raney Ni / ethanol / 6 h / 20 °C / 775.74 Torr

With sodium hydroxide; dimethylsulfide borane complex; hydrogen; chloroformic acid ethyl ester; acetic acid; triethylamine; trifluoroacetic acid; nickel; In 1,4-dioxane; methanol; ethanol; diethylene glycol dimethyl ether;
DOI:10.1021/jm011067f