C₂₆H₃₈O₅Si

Base Information Edit

Chemical Name:C₂₆H₃₈O₅Si
CAS No.:1443743-47-2
Molecular Formula:C₂₆H₃₈O₅Si
Molecular Weight:458.67
Hs Code.:
Mol file:1443743-47-2.mol

C<sub>26</sub>H<sub>38</sub>O<sub>5</sub>Si

Synonyms:C₂₆H₃₈O₅Si

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Chemical Property of C₂₆H₃₈O₅Si Edit

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Technology Process of C₂₆H₃₈O₅Si

There total 8 articles about C₂₆H₃₈O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1443743-53-0
C₂₇H₄₀O₄Si

: 1443743-47-2
C₂₆H₃₈O₅Si

Guidance literature:: C₂₇H₄₀O₄Si; With pyridine; ozone; In dichloromethane; at -78 ℃; Inert atmosphere;

With triphenylphosphine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol401367h

Reference yield:

: 203862-58-2
1,5-anhydro-2-deoxy-4,6-O-p-methoxybenzylidene-D-arabino-hexitol

: 1443743-47-2
C₂₆H₃₈O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C / Inert atmosphere

1.2: -15 - 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / toluene / 0.01 h / -78 - -10 °C / Inert atmosphere

3.1: triphenylphosphine; 1H-imidazole; iodine / tetrahydrofuran / 12 h / 55 °C / Inert atmosphere; Darkness

4.1: tert.-butyl lithium / tetrahydrofuran / 0.5 h / -78 - -60 °C / Inert atmosphere

4.2: -78 - 0 °C / Inert atmosphere

5.1: ozone; pyridine / dichloromethane / -78 °C / Inert atmosphere

5.2: -78 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; iodine; tert.-butyl lithium; sodium hydride; diisobutylaluminium hydride; ozone; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ol401367h

Reference yield:

: 3971-47-9,7103-29-9,13035-11-5,26242-03-5
(3S,4R)-dihydroxy-(2R)-(hydroxymethyl)tetrahydropyran

: 1443743-47-2
C₂₆H₃₈O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: camphor-10-sulfonic acid / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C / Inert atmosphere

2.2: -15 - 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / toluene / 0.01 h / -78 - -10 °C / Inert atmosphere

4.1: triphenylphosphine; 1H-imidazole; iodine / tetrahydrofuran / 12 h / 55 °C / Inert atmosphere; Darkness

5.1: tert.-butyl lithium / tetrahydrofuran / 0.5 h / -78 - -60 °C / Inert atmosphere

5.2: -78 - 0 °C / Inert atmosphere

6.1: ozone; pyridine / dichloromethane / -78 °C / Inert atmosphere

6.2: -78 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; camphor-10-sulfonic acid; iodine; tert.-butyl lithium; sodium hydride; diisobutylaluminium hydride; ozone; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ol401367h