4-benzyloxyquinoline-2-carboxylic acid [1(S)-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2-bromoethyl] ester

Base Information

Chemical Name:4-benzyloxyquinoline-2-carboxylic acid [1(S)-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2-bromoethyl] ester
CAS No.:798576-75-7
Molecular Formula:C₃₇H₃₀BrNO₇
Molecular Weight:680.552
Hs Code.:

Synonyms:4-benzyloxyquinoline-2-carboxylic acid [1(S)-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2-bromoethyl] ester

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Chemical Property of 4-benzyloxyquinoline-2-carboxylic acid [1(S)-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2-bromoethyl] ester

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Technology Process of 4-benzyloxyquinoline-2-carboxylic acid [1(S)-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2-bromoethyl] ester

There total 4 articles about 4-benzyloxyquinoline-2-carboxylic acid [1(S)-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2-bromoethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 52144-34-0
4-benzyloxyquinoline-2-carboxylic acid

: 104040-10-0
6-bromo-2,3-O,O-dibenzyl-L-ascorbic acid

: 798576-75-7
4-benzyloxyquinoline-2-carboxylic acid [1(S)-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2-bromoethyl] ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2004.07.043

Reference yield:

: 492-27-3
kinurenic acid

: 798576-75-7
4-benzyloxyquinoline-2-carboxylic acid [1(S)-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2-bromoethyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / H₂SO₄ / 24 h / Heating

2: K₂CO₃ / dimethylformamide / 4 h / Heating

3: 220 mg / NaOH / H₂O; methanol / 2 h / 20 °C

4: 60 percent / DMAP; DCC / CH₂Cl₂ / 20 °C

With dmap; sodium hydroxide; sulfuric acid; potassium carbonate; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.07.043

Reference yield:

: 5965-59-3
4-hydroxyquinoline-2-carboxylic acid methyl ester

: 798576-75-7
4-benzyloxyquinoline-2-carboxylic acid [1(S)-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2-bromoethyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / 4 h / Heating

2: 220 mg / NaOH / H₂O; methanol / 2 h / 20 °C

3: 60 percent / DMAP; DCC / CH₂Cl₂ / 20 °C

With dmap; sodium hydroxide; potassium carbonate; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.07.043