(Z)-N-(1-chloro-2,2,2-trifluoroethylidene)-2-cyclopropyl-5-nitrobenzenamine

Base Information

Chemical Name:(Z)-N-(1-chloro-2,2,2-trifluoroethylidene)-2-cyclopropyl-5-nitrobenzenamine
CAS No.:1356493-63-4
Molecular Formula:C₁₁H₈ClF₃N₂O₂
Molecular Weight:292.645
Hs Code.:

Synonyms:(Z)-N-(1-chloro-2,2,2-trifluoroethylidene)-2-cyclopropyl-5-nitrobenzenamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-N-(1-chloro-2,2,2-trifluoroethylidene)-2-cyclopropyl-5-nitrobenzenamine

Chemical Property:

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Technology Process of (Z)-N-(1-chloro-2,2,2-trifluoroethylidene)-2-cyclopropyl-5-nitrobenzenamine

There total 2 articles about (Z)-N-(1-chloro-2,2,2-trifluoroethylidene)-2-cyclopropyl-5-nitrobenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1239596-36-1
2-cyclopropyl-5-nitroaniline

: 76-05-1
trifluoroacetic acid

: 1356493-63-4
(Z)-N-(1-chloro-2,2,2-trifluoroethylidene)-2-cyclopropyl-5-nitrobenzenamine

Guidance literature:: trifluoroacetic acid; With tetrachloromethane; triethylamine; triphenylphosphine; at 0 ℃; for 0.166667h;

2-cyclopropyl-5-nitroaniline; for 12h; Reflux;

Reference yield:

: 10403-47-1
2-bromo 5-nitroaniline

: 1356493-63-4
(Z)-N-(1-chloro-2,2,2-trifluoroethylidene)-2-cyclopropyl-5-nitrobenzenamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: tricyclohexylphosphine; caesium carbonate / palladium diacetate / toluene; water / 12 h / Inert atmosphere; Reflux

2.1: triethylamine; triphenylphosphine; tetrachloromethane / 0.17 h / 0 °C

2.2: 12 h / Reflux

With tetrachloromethane; caesium carbonate; triethylamine; triphenylphosphine; tricyclohexylphosphine; palladium diacetate; In water; toluene;