11-{4-[(Z)-2-(1,3-benzodioxol-5-yl)-2-cyanoethenyl]-2-methoxyphenoxy}undecyl 3,5-diaminobenzoate

Base Information

Chemical Name:11-{4-[(Z)-2-(1,3-benzodioxol-5-yl)-2-cyanoethenyl]-2-methoxyphenoxy}undecyl 3,5-diaminobenzoate
CAS No.:1425539-76-9
Molecular Formula:C₃₅H₄₁N₃O₆
Molecular Weight:599.727
Hs Code.:

Synonyms:11-{4-[(Z)-2-(1,3-benzodioxol-5-yl)-2-cyanoethenyl]-2-methoxyphenoxy}undecyl 3,5-diaminobenzoate

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Chemical Property of 11-{4-[(Z)-2-(1,3-benzodioxol-5-yl)-2-cyanoethenyl]-2-methoxyphenoxy}undecyl 3,5-diaminobenzoate

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Technology Process of 11-{4-[(Z)-2-(1,3-benzodioxol-5-yl)-2-cyanoethenyl]-2-methoxyphenoxy}undecyl 3,5-diaminobenzoate

There total 4 articles about 11-{4-[(Z)-2-(1,3-benzodioxol-5-yl)-2-cyanoethenyl]-2-methoxyphenoxy}undecyl 3,5-diaminobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1425539-75-8
11-{4-[(Z)-2-(1,3-benzodioxol-5-yl)-2-cyanoethenyl]-2-methoxyphenoxy}undecyl 3,5-dinitrobenzoate

: 1425539-76-9
11-{4-[(Z)-2-(1,3-benzodioxol-5-yl)-2-cyanoethenyl]-2-methoxyphenoxy}undecyl 3,5-diaminobenzoate

Guidance literature:: With iron(III) chloride hexahydrate; zinc; In water; N,N-dimethyl-formamide; for 2.5h;

Reference yield: 61.0%

: iron (III) chloride hexahydrate

: 1425539-75-8
11-{4-[(Z)-2-(1,3-benzodioxol-5-yl)-2-cyanoethenyl]-2-methoxyphenoxy}undecyl 3,5-dinitrobenzoate

: 1425539-76-9
11-{4-[(Z)-2-(1,3-benzodioxol-5-yl)-2-cyanoethenyl]-2-methoxyphenoxy}undecyl 3,5-diaminobenzoate

Guidance literature:: In water; ethyl acetate; N,N-dimethyl-formamide; toluene;

Reference yield:

: 99-33-2
3,5-dinitrobenoyl chloride

: 1425539-76-9
11-{4-[(Z)-2-(1,3-benzodioxol-5-yl)-2-cyanoethenyl]-2-methoxyphenoxy}undecyl 3,5-diaminobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; pyridine / N,N-dimethyl-formamide; toluene; acetonitrile

2: N,N-dimethyl-formamide; water; toluene; ethyl acetate

With pyridine; dmap; In water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile;