2-Benzyl-1,2,4a,9-tetrahydro-cis-13bH-9,13b-methanodibenzo<3,4;6,7>cyclohepta<1,2-c>pyridin-3(4H)-one

Base Information

Chemical Name:2-Benzyl-1,2,4a,9-tetrahydro-cis-13bH-9,13b-methanodibenzo<3,4;6,7>cyclohepta<1,2-c>pyridin-3(4H)-one
CAS No.:72917-20-5
Molecular Formula:C₂₆H₂₃NO
Molecular Weight:365.475
Hs Code.:

Synonyms:2-Benzyl-1,2,4a,9-tetrahydro-cis-13bH-9,13b-methanodibenzo<3,4;6,7>cyclohepta<1,2-c>pyridin-3(4H)-one

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Chemical Property of 2-Benzyl-1,2,4a,9-tetrahydro-cis-13bH-9,13b-methanodibenzo<3,4;6,7>cyclohepta<1,2-c>pyridin-3(4H)-one

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Technology Process of 2-Benzyl-1,2,4a,9-tetrahydro-cis-13bH-9,13b-methanodibenzo<3,4;6,7>cyclohepta<1,2-c>pyridin-3(4H)-one

There total 3 articles about 2-Benzyl-1,2,4a,9-tetrahydro-cis-13bH-9,13b-methanodibenzo<3,4;6,7>cyclohepta<1,2-c>pyridin-3(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72917-19-2
2-Benzyl-1,2-dihydro-13bH-9,13b-methanodibenzo<3,4;6,7>cyclohepta<1,2-c>pyridin-3(9H)-one

: 72917-20-5
2-Benzyl-1,2,4a,9-tetrahydro-cis-13bH-9,13b-methanodibenzo<3,4;6,7>cyclohepta<1,2-c>pyridin-3(4H)-one

Guidance literature:: With palladium on activated charcoal; hydrogen; In tetrahydrofuran; acetic acid; for 84h; under 2585.7 Torr; Parr shaker;
DOI:10.1021/jo01296a032

Reference yield:

: 1197-51-9
N-propargylbenzylamine

: 72917-20-5
2-Benzyl-1,2,4a,9-tetrahydro-cis-13bH-9,13b-methanodibenzo<3,4;6,7>cyclohepta<1,2-c>pyridin-3(4H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) THF, pyridine, RT, 3 h, 2.) p-xylene, reflux, 90 min

2: 30.5 percent / p-Toluenesulfonic acid / acetic acid / 26 h / Heating

3: 10percent Pd/C, H₂ / tetrahydrofuran; acetic acid / 84 h / 2585.7 Torr / Parr shaker

With palladium on activated charcoal; hydrogen; toluene-4-sulfonic acid; In tetrahydrofuran; acetic acid;
DOI:10.1021/jo01296a032

Reference yield:

: 72917-18-1
C₂₆H₂₁NO

: 72917-20-5
2-Benzyl-1,2,4a,9-tetrahydro-cis-13bH-9,13b-methanodibenzo<3,4;6,7>cyclohepta<1,2-c>pyridin-3(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 30.5 percent / p-Toluenesulfonic acid / acetic acid / 26 h / Heating

2: 10percent Pd/C, H₂ / tetrahydrofuran; acetic acid / 84 h / 2585.7 Torr / Parr shaker

With palladium on activated charcoal; hydrogen; toluene-4-sulfonic acid; In tetrahydrofuran; acetic acid;
DOI:10.1021/jo01296a032