Technology Process of C23H34O2
There total 6 articles about C23H34O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C20H29IO2; allylmagnesium bromide;
With
N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide;
In
tetrahydrofuran;
at -40 ℃;
In
tetrahydrofuran;
at 0 - 20 ℃;
DOI:10.1039/c2cc36260k
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: chloro-trimethyl-silane; pyridine / tetrahydrofuran / -78 °C
1.2: -78 - 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 0 - 20 °C / Reflux
3.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere
4.1: sodium iodide / butanone / 24 h / Reflux
5.1: copper(l) iodide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / -40 °C
5.2: 0 - 20 °C
With
pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; lithium aluminium tetrahydride; chloro-trimethyl-silane; triethylamine; sodium iodide;
In
tetrahydrofuran; dichloromethane; butanone;
DOI:10.1039/c2cc36260k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere
2.1: sodium iodide / butanone / 24 h / Reflux
3.1: copper(l) iodide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / -40 °C
3.2: 0 - 20 °C
With
N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; triethylamine; sodium iodide;
In
tetrahydrofuran; dichloromethane; butanone;
DOI:10.1039/c2cc36260k
