S-Benzyl-β-mercaptopropionyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteinyl-prolyl-N^G-p-toluenesulfonyl-D-arginine Benzyl Ester

Base Information

• Chemical Name: S-Benzyl-β-mercaptopropionyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteinyl-prolyl-N^G-p-toluenesulfonyl-D-arginine Benzyl Ester
• CAS No.: 89137-88-2
• Molecular Formula: C₇₂H₈₆N₁₂O₁₄S₃
• Molecular Weight: 1439.74

Synonyms:S-Benzyl-β-mercaptopropionyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteinyl-prolyl-N^G-p-toluenesulfonyl-D-arginine Benzyl Ester

Chemical Property of S-Benzyl-β-mercaptopropionyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteinyl-prolyl-N^G-p-toluenesulfonyl-D-arginine Benzyl Ester

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Technology Process of S-Benzyl-β-mercaptopropionyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteinyl-prolyl-N^G-p-toluenesulfonyl-D-arginine Benzyl Ester

There total 1 articles about S-Benzyl-β-mercaptopropionyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteinyl-prolyl-N^G-p-toluenesulfonyl-D-arginine Benzyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

o-Nitrobenzenesulfenylprolyl-NG-p-toluenesulfonyl-D-arginine Benzyl Ester (88681-56-5) + S-Benzyl-β-mercaptopropionyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine Azide → S-Benzyl-β-mercaptopropionyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteinyl-prolyl-NG-p-toluenesulfonyl-D-arginine Benzyl Ester (89137-88-2)

Guidance literature:

In N,N-dimethyl-formamide; at 0 ℃; for 72h; Label V used as hydrochloride;

DOI:10.1135/cccc19832862

Reference yield:

S-Benzyl-β-mercaptopropionyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteinyl-prolyl-NG-p-toluenesulfonyl-D-arginine Benzyl Ester (89137-88-2) → Cyclic Disulfide of β-Mercaptopropionyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-cysteinyl-prolyl-D-arginine (84236-22-6)

Guidance literature:

With sodium; potassium hexacyanoferrate(III); Yield given. Multistep reaction; 1) Liquid NH₃ 2) 0.01 M HCl, 1 h;

DOI:10.1135/cccc19832862

upstream raw materials:

o-Nitrobenzenesulfenylprolyl-N^G-p-toluenesulfonyl-D-arginine Benzyl Ester

Downstream raw materials:

Cyclic Disulfide of β-Mercaptopropionyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-cysteinyl-prolyl-D-arginine

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