Technology Process of C24H36O7
There total 3 articles about C24H36O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C22H29NO6;
With
cerium(III) chloride heptahydrate;
In
methanol;
at 20 ℃;
for 0.75h;
Inert atmosphere;
With
sodium tetrahydroborate;
In
methanol;
at -78 ℃;
for 1.08333h;
Inert atmosphere;
chloromethyl methyl ether;
With
dmap; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1021/jo2010389
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.67 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 °C / Inert atmosphere
2.1: caesium carbonate / acetonitrile / 0.75 h / 20 °C / Inert atmosphere
2.2: 1 h / 0 °C / Inert atmosphere
3.1: cerium(III) chloride heptahydrate / methanol / 0.75 h / 20 °C / Inert atmosphere
3.2: 1.08 h / -78 °C / Inert atmosphere
3.3: 0 - 20 °C / Inert atmosphere
With
cerium(III) chloride heptahydrate; caesium carbonate; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; acetonitrile;
2.1: Horner-Wadsworth-Emmons olefination / 2.2: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/jo2010389
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: caesium carbonate / acetonitrile / 0.75 h / 20 °C / Inert atmosphere
1.2: 1 h / 0 °C / Inert atmosphere
2.1: cerium(III) chloride heptahydrate / methanol / 0.75 h / 20 °C / Inert atmosphere
2.2: 1.08 h / -78 °C / Inert atmosphere
2.3: 0 - 20 °C / Inert atmosphere
With
cerium(III) chloride heptahydrate; caesium carbonate;
In
methanol; acetonitrile;
1.1: Horner-Wadsworth-Emmons olefination / 1.2: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/jo2010389
