5-bromo-5'-trityl-2'-deoxyuridine 3'-ethyl>glycyl ester>

Base Information

Chemical Name:5-bromo-5'-trityl-2'-deoxyuridine 3'-ethyl>glycyl ester>
CAS No.:130327-98-9
Molecular Formula:C₄₄H₅₃BrN₄O₁₀
Molecular Weight:877.83
Hs Code.:

5-bromo-5'-trityl-2'-deoxyuridine 3'-<N-(1,1-dimethylethoxycarbonyl)-N-<2-<N-(1,1-dimethylethoxycarbonyl)-N-ethylamino>ethyl>glycyl ester>

Synonyms:5-bromo-5'-trityl-2'-deoxyuridine 3'-ethyl>glycyl ester>

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Chemical Property of 5-bromo-5'-trityl-2'-deoxyuridine 3'-ethyl>glycyl ester>

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Technology Process of 5-bromo-5'-trityl-2'-deoxyuridine 3'-ethyl>glycyl ester>

There total 4 articles about 5-bromo-5'-trityl-2'-deoxyuridine 3'-ethyl>glycyl ester> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 130327-93-4
N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine

: 15414-60-5
5-bromo-5'-O-trityl-2'-deoxyuridine

: 130327-98-9
5-bromo-5'-trityl-2'-deoxyuridine 3'-ethyl>glycyl ester>

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 25 ℃;
DOI:10.1021/jm00171a038

Reference yield: 48.0%

: 130327-94-5
N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine N-succinimide ester

: 15414-60-5
5-bromo-5'-O-trityl-2'-deoxyuridine

: 130327-98-9
5-bromo-5'-trityl-2'-deoxyuridine 3'-ethyl>glycyl ester>

Guidance literature:: With dmap; In acetonitrile; for 120h; Ambient temperature;
DOI:10.1021/jm00171a038

Reference yield:

: 76-83-5
trityl chloride

: 130327-98-9
5-bromo-5'-trityl-2'-deoxyuridine 3'-ethyl>glycyl ester>

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / pyridine / 1 h / 120 °C

2: 100 percent / 4-(dimethylamino)pyridine, dicyclohexylcarbodiimide / CH₂Cl₂ / 0 - 25 °C

With pyridine; dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm00171a038