phenyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:phenyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-1-thio-α-D-mannopyranoside
CAS No.:1083236-97-8
Molecular Formula:C₃₈H₄₂O₇S
Molecular Weight:642.813
Hs Code.:

Synonyms:phenyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-1-thio-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-1-thio-α-D-mannopyranoside

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Technology Process of phenyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-1-thio-α-D-mannopyranoside

There total 1 articles about phenyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 316188-24-6
phenyl 2,3,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 1083236-97-8
phenyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-1-thio-α-D-mannopyranoside

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jo801630m

Reference yield: 59.0%

: 516-12-1
N-iodo-succinimide

: 1083236-97-8
phenyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-1-thio-α-D-mannopyranoside

: 1083236-99-0
N-( 2',3',6'-tri-O-benzyl-4'-O-tert-butyloxycarbonyl-α-D-mannopyranosyl)succinimide

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; at -10 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo801630m

Reference yield:

: 1083236-97-8
phenyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-1-thio-α-D-mannopyranoside

: 67-63-0,8013-70-5
isopropyl alcohol

: 1083237-14-2
isopropyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-β-D-mannopyranoside

: 1083236-98-9
isopropyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-α-D-mannopyranoside

Guidance literature:: phenyl 2,3,6-tri-O-benzyl-4-O-tert-butyloxycarbonyl-1-thio-α-D-mannopyranoside; With 1-(phenylsulfonyl)piperidine; 2,4,5-tri-tert-butylpyrimidine; In dichloromethane; at -40 ℃; Molecular sieve; Inert atmosphere;

isopropyl alcohol; In dichloromethane; at -40 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jo801630m