phthalic acid (2S,3S)-N-3(2-phenylthietanyl)monoamid

Base Information

Chemical Name:phthalic acid (2S,3S)-N-3(2-phenylthietanyl)monoamid
CAS No.:158868-60-1
Molecular Formula:C₁₇H₁₅NO₃S
Molecular Weight:313.377
Hs Code.:

Synonyms:phthalic acid (2S,3S)-N-3(2-phenylthietanyl)monoamid

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Chemical Property of phthalic acid (2S,3S)-N-3(2-phenylthietanyl)monoamid

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Technology Process of phthalic acid (2S,3S)-N-3(2-phenylthietanyl)monoamid

There total 2 articles about phthalic acid (2S,3S)-N-3(2-phenylthietanyl)monoamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 123475-41-2
(1S,2S)-1-phenyl-2-phthalimido-1,3-propanediol ditosyl ester

: 158868-60-1
phthalic acid (2S,3S)-N-3(2-phenylthietanyl)monoamid

Guidance literature:: With potassium ethyl xanthogenate; In acetone; for 48h; Heating;
DOI:10.1016/0957-4166(94)80174-6

Reference yield:

: 123537-84-8
(1S,2S)-1-phenyl-2-phthalimido-propane-1,3-diol

: 158868-60-1
phthalic acid (2S,3S)-N-3(2-phenylthietanyl)monoamid

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridine / 144 h / Ambient temperature

2: 80 percent / potassium O-ethyldithiocarbonate / acetone / 48 h / Heating

With pyridine; potassium ethyl xanthogenate; In acetone;
DOI:10.1016/0957-4166(94)80174-6

Reference yield:

: 158868-60-1
phthalic acid (2S,3S)-N-3(2-phenylthietanyl)monoamid

: (2S,3S)-3-amino-2-phenylthietane

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride, pyridine / 18 h / Ambient temperature

2: 80percent aq. hydrazine / butan-1-ol / 2 h / Heating

With pyridine; acetic anhydride; hydrazine hydrate; In butan-1-ol;
DOI:10.1016/0957-4166(94)80174-6