C₁₃H₂₃IO₂Si

Base Information

Chemical Name:C₁₃H₂₃IO₂Si
CAS No.:1198227-66-5
Molecular Formula:C₁₃H₂₃IO₂Si
Molecular Weight:366.314
Hs Code.:

C<sub>13</sub>H<sub>23</sub>IO<sub>2</sub>Si

Synonyms:C₁₃H₂₃IO₂Si

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Chemical Property of C₁₃H₂₃IO₂Si

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Technology Process of C₁₃H₂₃IO₂Si

There total 6 articles about C₁₃H₂₃IO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1198227-64-3
C₁₄H₂₅IO₃Si

: 1198227-66-5
C₁₃H₂₃IO₂Si

: 1198227-65-4
C₁₃H₂₅IO₂Si

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃; for 1h;

Reference yield: 85.0%

: 1198227-65-4
C₁₃H₂₅IO₂Si

: 1198227-66-5
C₁₃H₂₃IO₂Si

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 1198227-61-0
C₁₁H₁₆O₃

: 1198227-66-5
C₁₃H₂₃IO₂Si

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; iodine / tetrachloromethane / 24 h / 50 °C

2: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 1.5 h / 0 °C

3: 1H-imidazole / dichloromethane / 1 h / 0 °C

4: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C

With pyridine; 1H-imidazole; sodium tetrahydroborate; cerium(III) chloride heptahydrate; iodine; diisobutylaluminium hydride; In methanol; tetrachloromethane; dichloromethane; toluene;