2,2-dimethylpropionic acid (Z)-11-{(1R,2R)-2-[(S)-3-(tert-butyldimethylsilanyloxy)-1-methylpropyl]cyclopropyl}undec-10-enyl ester

Base Information

Chemical Name:2,2-dimethylpropionic acid (Z)-11-{(1R,2R)-2-[(S)-3-(tert-butyldimethylsilanyloxy)-1-methylpropyl]cyclopropyl}undec-10-enyl ester
CAS No.:1446326-59-5
Molecular Formula:C₃₉H₆₀O₃Si
Molecular Weight:604.989
Hs Code.:

Synonyms:2,2-dimethylpropionic acid (Z)-11-{(1R,2R)-2-[(S)-3-(tert-butyldimethylsilanyloxy)-1-methylpropyl]cyclopropyl}undec-10-enyl ester

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Chemical Property of 2,2-dimethylpropionic acid (Z)-11-{(1R,2R)-2-[(S)-3-(tert-butyldimethylsilanyloxy)-1-methylpropyl]cyclopropyl}undec-10-enyl ester

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Technology Process of 2,2-dimethylpropionic acid (Z)-11-{(1R,2R)-2-[(S)-3-(tert-butyldimethylsilanyloxy)-1-methylpropyl]cyclopropyl}undec-10-enyl ester

There total 1 articles about 2,2-dimethylpropionic acid (Z)-11-{(1R,2R)-2-[(S)-3-(tert-butyldimethylsilanyloxy)-1-methylpropyl]cyclopropyl}undec-10-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 918905-62-1
trans-(1S,2R)-2-[(S)-3-(tert-butyldiphenylsilanyloxy)-1-methylpropyl]cyclopropanecarbaldehyde

: 1192146-31-8
2,2-dimethylpropionic acid 10-(1-phenyl-1H-tetrazole-5-sulfonyl)decyl ester

: 1446326-58-4
2,2-dimethylpropionic acid (E)-11-{(1R,2R)-2-[(S)-3-(tert-butyldimethylsilanyloxy)-1-methylpropyl]cyclopropyl}undec-10-enyl ester

: 1446326-59-5
2,2-dimethylpropionic acid (Z)-11-{(1R,2R)-2-[(S)-3-(tert-butyldimethylsilanyloxy)-1-methylpropyl]cyclopropyl}undec-10-enyl ester

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; for 2h; Overall yield = 85 %; Overall yield = 5.55 g;
DOI:10.1016/j.tet.2013.04.134