2-(6-methoxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)prop-2-enenitrile (non-preferred name)

Base Information Edit

Chemical Name:2-(6-methoxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)prop-2-enenitrile (non-preferred name)
CAS No.:83905-33-3
Molecular Formula:C11H15 N O4
Molecular Weight:225.2411
Hs Code.:
Mol file:83905-33-3.mol

Synonyms:Furo[2,3-d]-1,3-dioxole,a-D-xylo-hexofuranurononitrilederiv.; NSC 356480

Suppliers and Price of 2-(6-methoxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)prop-2-enenitrile (non-preferred name)

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(6-methoxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)prop-2-enenitrile (non-preferred name) Edit

Chemical Property:

Vapor Pressure:0.000189mmHg at 25°C
Boiling Point:328.5°Cat760mmHg
Flash Point:132.1°C
Density:1.18g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(6-methoxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)prop-2-enenitrile (non-preferred name)

There total 2 articles about 2-(6-methoxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)prop-2-enenitrile (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 71485-92-2
(3aR,5R,6S,6aR)-6-methoxy-2,2-dimethyl-5-((E)-2-nitrovinyl)tetrahydrofuro[2,3-d][1,3]dioxole

: 57-12-5
cyanide^(1-)

: 83905-33-3
5,6-Dideoxy-1,2-O-isopropylidene-3-O-methyl-5-C-methylene-α-D-xylo-hexofuranurononitrile

Guidance literature:: DOI:10.1002/hlca.19820650512

Reference yield:

: 71485-92-2
(3aR,5R,6S,6aR)-6-methoxy-2,2-dimethyl-5-((E)-2-nitrovinyl)tetrahydrofuro[2,3-d][1,3]dioxole

: 151-50-8
potassium cyanide

: 83905-33-3
5,6-Dideoxy-1,2-O-isopropylidene-3-O-methyl-5-C-methylene-α-D-xylo-hexofuranurononitrile

Guidance literature:: With hydrogenchloride; tetrabutylammomium bromide; triethylamine; Yield given. Multistep reaction; 1.) toluene, water, r.t., 18 h; 2.) 80 deg C, 3 h;