5-(4-carboxyphenyl)-15-(4-carbomethoxyphenyl)-10,20-bis(2,4,6-trimethylphenyl) porphyrin

Base Information

• Chemical Name: 5-(4-carboxyphenyl)-15-(4-carbomethoxyphenyl)-10,20-bis(2,4,6-trimethylphenyl) porphyrin
• CAS No.: 394736-99-3
• Molecular Formula: C₅₃H₄₄N₄O₄
• Molecular Weight: 800.957

Synonyms:5-(4-carboxyphenyl)-15-(4-carbomethoxyphenyl)-10,20-bis(2,4,6-trimethylphenyl) porphyrin

Chemical Property of 5-(4-carboxyphenyl)-15-(4-carbomethoxyphenyl)-10,20-bis(2,4,6-trimethylphenyl) porphyrin

Chemical Property:

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Technology Process of 5-(4-carboxyphenyl)-15-(4-carbomethoxyphenyl)-10,20-bis(2,4,6-trimethylphenyl) porphyrin

There total 3 articles about 5-(4-carboxyphenyl)-15-(4-carbomethoxyphenyl)-10,20-bis(2,4,6-trimethylphenyl) porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(mesityl)dipyrromethane (159152-14-4) → 5-(4-carboxyphenyl)-15-(4-carbomethoxyphenyl)-10,20-bis(2,4,6-trimethylphenyl) porphyrin (394736-99-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone

2: trifluoroacetic acid; hydrogenchloride / liquid HCl

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In hydrogenchloride; trifluoroacetic acid;

DOI:10.1039/c3dt50711d

Reference yield:

methyl 4-formylbenzoate (1571-08-0) → 5-(4-carboxyphenyl)-15-(4-carbomethoxyphenyl)-10,20-bis(2,4,6-trimethylphenyl) porphyrin (394736-99-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone

2: trifluoroacetic acid; hydrogenchloride / liquid HCl

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In hydrogenchloride; trifluoroacetic acid;

DOI:10.1039/c3dt50711d

Reference yield:

10,20-bis(2,4,6-trimethylphenyl)-5,15-bis(4-carbomethoxyphenyl) porphyrin (394736-98-2) → 5-(4-carboxyphenyl)-15-(4-carbomethoxyphenyl)-10,20-bis(2,4,6-trimethylphenyl) porphyrin (394736-99-3)

Guidance literature:

In hydrogenchloride; trifluoroacetic acid; liquid HCl;

DOI:10.1039/c3dt50711d

upstream raw materials:

10,20-bis(2,4,6-trimethylphenyl)-5,15-bis(4-carbomethoxyphenyl) porphyrin

5-(mesityl)dipyrromethane

methyl 4-formylbenzoate

Downstream raw materials:

C₉₉H₇₃F₂N₉O₅

C₁₀₁H₇₃F₆N₉O₅

[5-(4-methoxycarbonylphenyl)-15-(4-aminophenyl)-10,20-bis(2,4,6-trimethylphenyl)porphyrin]

15-(4-carbomethoxyphenyl)-5-(N-tert-butoxycarbonyl-4-aminophenyl)-10,20-bis(2,3,4,5,6-pentafluorophenyl) porphyrin

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