(E)-1-<4-(n-Hexadecyloxy)phenyl>-2-(N-methyl-4-pyridinio)ethene iodide

Base Information

• Chemical Name: (E)-1-<4-(n-Hexadecyloxy)phenyl>-2-(N-methyl-4-pyridinio)ethene iodide
• CAS No.: 90990-84-4
• Molecular Formula: C₃₀H₄₆NO*I
• Molecular Weight: 563.606
• Mol file: 90990-84-4.mol

Synonyms:(E)-1-<4-(n-Hexadecyloxy)phenyl>-2-(N-methyl-4-pyridinio)ethene iodide

Chemical Property of (E)-1-<4-(n-Hexadecyloxy)phenyl>-2-(N-methyl-4-pyridinio)ethene iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-1-<4-(n-Hexadecyloxy)phenyl>-2-(N-methyl-4-pyridinio)ethene iodide

There total 3 articles about (E)-1-<4-(n-Hexadecyloxy)phenyl>-2-(N-methyl-4-pyridinio)ethene iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.5%

p-n-hexadecyloxybenzaldehyde (59117-18-9) + N-methyl-4-methylpyridinium iodide (2301-80-6) → (E)-1-<4-(n-Hexadecyloxy)phenyl>-2-(N-methyl-4-pyridinio)ethene iodide (90990-84-4)

Guidance literature:

With piperidine;

DOI:10.1021/jo00191a009

Reference yield:

1-iodohexadecane (544-77-4) → (E)-1-<4-(n-Hexadecyloxy)phenyl>-2-(N-methyl-4-pyridinio)ethene iodide (90990-84-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 95.1 percent / 1) Cs₂CO₃ / 1) Cs₂CO₃, MeOH 2) DMF

2: 34.5 percent / piperidine

With piperidine; caesium carbonate;

DOI:10.1021/jo00191a009

Reference yield:

4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → (E)-1-<4-(n-Hexadecyloxy)phenyl>-2-(N-methyl-4-pyridinio)ethene iodide (90990-84-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 95.1 percent / 1) Cs₂CO₃ / 1) Cs₂CO₃, MeOH 2) DMF

2: 34.5 percent / piperidine

With piperidine; caesium carbonate;

DOI:10.1021/jo00191a009

upstream raw materials:

p-n-hexadecyloxybenzaldehyde

N-methyl-4-methylpyridinium iodide

1-iodohexadecane

4-hydroxy-benzaldehyde