C₂₂H₂₃N₃O₄S

Base Information

Chemical Name:C₂₂H₂₃N₃O₄S
CAS No.:1312435-61-2
Molecular Formula:C₂₂H₂₃N₃O₄S
Molecular Weight:425.508
Hs Code.:

C<sub>22</sub>H<sub>23</sub>N<sub>3</sub>O<sub>4</sub>S

Synonyms:C₂₂H₂₃N₃O₄S

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Chemical Property of C₂₂H₂₃N₃O₄S

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Technology Process of C₂₂H₂₃N₃O₄S

There total 3 articles about C₂₂H₂₃N₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 40052-13-9
mono-tert-butyl malonate

: 1221919-68-1
2-(6-phenylbenzo[d]thiazol-2-yl)acetohydrazide

: 1312435-61-2
C₂₂H₂₃N₃O₄S

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 14h; Inert atmosphere;

Reference yield:

: 791614-78-3
ethyl 2-(6-bromobenzo[d]thiazol-2-yl)acetate

: 1312435-61-2
C₂₂H₂₃N₃O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 6 h / Reflux

2: hydrazine hydrate / 1-methyl-pyrrolidin-2-one / 7 h / 95 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 14 h / 20 °C / Inert atmosphere

With potassium phosphate; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide;

Reference yield:

: 80945-86-4
6-bromo-2-chloro-benzothiazole

: 1312435-61-2
C₂₂H₂₃N₃O₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hexamethyldisilazane / toluene; tetrahydrofuran / 1.17 h / -60 °C / Inert atmosphere

1.2: 2 h / 0 °C

2.1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 6 h / Reflux

3.1: hydrazine hydrate / 1-methyl-pyrrolidin-2-one / 7 h / 95 °C

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 14 h / 20 °C / Inert atmosphere

With potassium phosphate; sodium hexamethyldisilazane; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide; toluene;