ethyl 2-(cyclohex-1-enyl)-1-(dimethylcarbamoyl)-1H-indole-3-carboxylate

Base Information

Chemical Name:ethyl 2-(cyclohex-1-enyl)-1-(dimethylcarbamoyl)-1H-indole-3-carboxylate
CAS No.:1275466-58-4
Molecular Formula:C₂₀H₂₄N₂O₃
Molecular Weight:340.422
Hs Code.:

Synonyms:ethyl 2-(cyclohex-1-enyl)-1-(dimethylcarbamoyl)-1H-indole-3-carboxylate

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Chemical Property of ethyl 2-(cyclohex-1-enyl)-1-(dimethylcarbamoyl)-1H-indole-3-carboxylate

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Technology Process of ethyl 2-(cyclohex-1-enyl)-1-(dimethylcarbamoyl)-1H-indole-3-carboxylate

There total 2 articles about ethyl 2-(cyclohex-1-enyl)-1-(dimethylcarbamoyl)-1H-indole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 101-42-8
fenuron

: ethyl 3-(cyclohex-1-en-1-yl)propiolate

: 1275466-58-4
ethyl 2-(cyclohex-1-enyl)-1-(dimethylcarbamoyl)-1H-indole-3-carboxylate

Guidance literature:: With tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; copper(II) acetate monohydrate; In toluene; at 60 ℃; for 18.5h; regioselective reaction;
DOI:10.1002/anie.201006381

Reference yield:

: 103-71-9
phenyl isocyanate

: 1275466-58-4
ethyl 2-(cyclohex-1-enyl)-1-(dimethylcarbamoyl)-1H-indole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; copper(II) acetate monohydrate / toluene / 18.5 h / 60 °C

With tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; copper(II) acetate monohydrate; triethylamine; In dichloromethane; toluene;
DOI:10.1002/anie.201006381

Reference yield: 99.0%

: 1275466-58-4
ethyl 2-(cyclohex-1-enyl)-1-(dimethylcarbamoyl)-1H-indole-3-carboxylate

: 1275467-04-3
ethyl 2-cyclohexyl-1-(dimethylcarbamoyl)-1H-indole-3-carboxylate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 80 ℃; for 16h; under 760.051 Torr;
DOI:10.1002/anie.201006381