thioacetic acid S-{3-bromo-4-[(diethoxyphosphoryl)difluoromethyl]benzyl} ester

Base Information

• Chemical Name: thioacetic acid S-{3-bromo-4-[(diethoxyphosphoryl)difluoromethyl]benzyl} ester
• CAS No.: 362527-65-9
• Molecular Formula: C₁₄H₁₈BrF₂O₄PS
• Molecular Weight: 431.235

Synonyms:thioacetic acid S-{3-bromo-4-[(diethoxyphosphoryl)difluoromethyl]benzyl} ester

Chemical Property of thioacetic acid S-{3-bromo-4-[(diethoxyphosphoryl)difluoromethyl]benzyl} ester

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Technology Process of thioacetic acid S-{3-bromo-4-[(diethoxyphosphoryl)difluoromethyl]benzyl} ester

There total 1 articles about thioacetic acid S-{3-bromo-4-[(diethoxyphosphoryl)difluoromethyl]benzyl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

potassium thioacetate (10387-40-3) + [(2-bromo-4-(bromomethyl)phenyl)difluoromethyl]phosphonic acid diethyl ester (362527-60-4) → thioacetic acid S-{3-bromo-4-[(diethoxyphosphoryl)difluoromethyl]benzyl} ester (362527-65-9)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

DOI:10.1016/j.bmc.2008.05.062

Reference yield: 96.0%

4-bromo-4'-(bromomethyl)biphenyl-3-sulfonic acid amide (1061617-69-3) + thioacetic acid S-{3-bromo-4-[(diethoxyphosphoryl)difluoromethyl]benzyl} ester (362527-65-9) → {[2-bromo-4-(4'-bromo-3'-sulfamoylbiphenyl-4-ylmethylsulfanylmethyl)phenyl]difluoromethyl}phosphonic acid diethyl ester (1061618-05-0)

Guidance literature:

With sodium hydroxide; In ethanol; chloroform; for 0.5h; cooling;

DOI:10.1016/j.bmc.2008.05.062

Reference yield: 72.0%

(4-bromo-4'-bromomethylbiphenyl-3-yl)difluoromethanesulfonamide (1061617-70-6) + thioacetic acid S-{3-bromo-4-[(diethoxyphosphoryl)difluoromethyl]benzyl} ester (362527-65-9) → ([2-bromo-4-(4'-bromo-3'-(sulfamoyldifluoromethyl)biphenyl-4-ylmethylsulfanylmethyl)phenyl]difluoromethyl)phosphonic acid diethyl ester (1061618-08-3)

Guidance literature:

With sodium hydroxide; In ethanol; chloroform; for 0.5h; cooling;

DOI:10.1016/j.bmc.2008.05.062

upstream raw materials:

potassium thioacetate

[(2-bromo-4-(bromomethyl)phenyl)difluoromethyl]phosphonic acid diethyl ester

Downstream raw materials:

{[2-bromo-4-(4'-bromo-3'-sulfamoylbiphenyl-4-ylmethylsulfanylmethyl)phenyl]difluoromethyl}phosphonic acid diethyl ester

([2-bromo-4-(4'-bromo-3'-(sulfamoyldifluoromethyl)biphenyl-4-ylmethylsulfanylmethyl)phenyl]difluoromethyl)phosphonic acid diethyl ester

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